Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,4 +1,4 @@ 1 -[[image:attach:TapeDrive_beschriftet.PNG||height=" 400"]][[image:attach:TapeDrive scheme.png||height="400"]]1 +[[image:attach:TapeDrive_beschriftet.PNG||height="250"]][[image:attach:TapeDrive scheme.png||height="250"]] 2 2 3 3 **14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)** 4 4 ... ... @@ -58,91 +58,20 @@ 58 58 59 59 * filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube 60 60 61 -[[image:attach:20211201_095534.jpg||height="250"]] 62 - 63 63 \\ 64 64 65 -**14.3 Connecting sample to ElveFlow, sample exchange 66 -** 67 - 68 -[[image:attach:20211201_095033.jpg||thumbnail="true" height="250"]][[image:attach:20211201_095205.jpg||height="250"]][[image:attach:20211201_095232.jpg||height="250"]] 69 - 70 70 \\ 71 71 72 - \\65 +**14.3 Connecting sample to ElveFlow** 73 73 74 -**14.4 TapeDrive operation 75 -** 76 - 77 -The TapeDrive is controlled through kamzik. To open kamzik, start the server. A terminal will open and shortly after a small window. 78 -Now start the client. Same thing, a terminal will open, shortly after a small window. 79 - 80 -Click 'Devices' in the **client session** to open the control window. 81 -[[image:attach:screen.PNG||height="250"]][[image:attach:server client.PNG||height="250"]] 82 - 83 -* **Tape:** 84 -** Click on the 'main tape' icon 85 -** Change the velocity by typing anything from **0.3-3.0 mm/s** 86 -** Common velocity is 1.0-1.5 mm/s 87 -** kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point. 88 88 \\ 89 -** [[image:attach:kamzik_tape.PNG||height="400"]] 90 90 91 91 \\ 92 92 93 -* **Sample nozzle:** 94 -** Click an the 'nozzle' icon. 95 -** ((( 96 -The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully. 97 -The absolute position is **not calibrated** and therefore changes after each restart of kamzik. 98 -\\(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 99 -\\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 100 - 101 -(% class="wrapped" %) 102 -|=((( 103 103 \\ 104 -)))|=((( 105 -direction 106 -)))|=((( 107 -recommended step size 108 -for visual adjustment 109 -)))|=(% colspan="1" %)((( 110 -recommended step size 111 -during data collection 112 -))) 113 -|((( 114 -+x 115 -)))|((( 116 -away from X-ray interaction point 117 -)))|((( 118 -1.0 - 0.5 mm 119 -)))|(% colspan="1" %)((( 120 -0.1 - 0.2 mm 121 -))) 122 -|((( 123 -+y 124 -)))|((( 125 -up 126 -)))|((( 127 -1.0 - 0.5 mm 128 -)))|(% colspan="1" %)((( 129 -0.1 - 0.2 mm 130 -))) 131 -|((( 132 -+z 133 -)))|((( 134 -towards detector tower, away from tape 135 -)))|((( 136 -0.5 - 0.2 mm 137 -)))|(% colspan="1" %)((( 138 -0.1 - 0.2 mm 139 -be careful with -z, tape could be pushed out of focus 140 -))) 141 141 73 +**14.4 TapeDrive operation 142 142 ** 143 -\\** 144 -))) 145 -** [[image:attach:kamzik_nozzle.PNG||height="400"]] 146 146 147 147 \\ 148 148 ... ... @@ -150,35 +150,6 @@ 150 150 151 151 \\ 152 152 153 -Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 154 - 155 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 156 - password: //written on control laptop (changes every 6 months) 157 -// 158 - 159 159 \\ 160 160 161 161 \\ 162 - 163 -**14.5 Tape roll exchange** 164 - 165 -The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s). 166 - 167 -* Remove the (almost) empty feeder roll by pulling it upwards. 168 -* Cut the tape with some cm overlap to glue to the new roll. 169 -* Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm** 170 -* Cut the first cm of the new tape roll, directly before the black sticky part. 171 -* Use this sticky part to attach the end of the old 172 - 173 -**[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]] 174 -** 175 - 176 -\\ 177 - 178 -\\ 179 - 180 -\\ 181 - 182 -\\ 183 - 184 -\\
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... ... @@ -1,1 +1,1 @@ 1 -23503 93981 +235034346 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/23503 9398/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/235034346/14. Serial Crystallography: CFEL TapeDrive