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Last modified by chatzies on 2025-11-27 11:35
From version 22.1
edited by ahenkel
on 2021-12-03 11:26
Change comment: There is no comment for this version
To version 23.1
edited by ahenkel
on 2021-12-03 11:32
Change comment: There is no comment for this version

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1 1  [[image:attach:TapeDrive_beschriftet.PNG||height="400"]][[image:attach:TapeDrive scheme.png||height="400"]]
2 2  
3 -**14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)**
3 +\\
4 4  
5 +\\
6 +
7 +\\
8 +
9 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1RevertfromCrystallographytoTapeDrive(P11staff/CFEL)"/}}**14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)** ===
10 +
5 5  * remove vortex
6 6  * beamstop to out-position?
7 7  * remove goniometer. The airbearing should be stopped (p11/servermotor/eh.1.01)
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50 50  
51 51  \\
52 52  
53 -**14.2 Sample characteristics and preparation**
59 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2Samplecharacteristicsandpreparation"/}}**14.2 Sample characteristics and preparation** ===
54 54  
55 55  suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
56 56  
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62 62  
63 63  \\
64 64  
65 -**14.3 Connecting sample to ElveFlow, sample exchange
66 -**
71 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3ConnectingsampletoElveFlow,sampleexchange"/}}**14.3 Connecting sample to ElveFlow, sample exchange
72 +** ===
67 67  
68 68  After filtration, screw the ElveFlow connector to your Eppendorf or Falcon tube. Make sure that the yellow-ish line goes to the bottom of your tube. You can adjust the length by unscrewing the blue fitting on top and pushing/pulling the yellow-ish line. **Don't forget to tigthen the blue fitting afterwards!**
69 69  
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79 79  
80 80  \\
81 81  
82 -**14.4 TapeDrive operation
83 -**
88 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4TapeDriveoperation"/}}**14.4 TapeDrive operation
89 +** ===
84 84  
85 85  The TapeDrive is controlled through kamzik. To open kamzik, start the server. A terminal will open and shortly after a small window.
86 86  Now start the client. Same thing, a terminal will open, shortly after a small window.
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88 88  Click 'Devices' in the **client session** to open the control window.
89 89  [[image:attach:screen.PNG||height="250"]][[image:attach:server client.PNG||height="250"]]
90 90  
91 -* **Tape:**
92 -** Click on the 'main tape' icon
93 -** Change the velocity by typing anything from **0.3-3.0 mm/s**
94 -** Common velocity is 1.0-1.5 mm/s
95 -** kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
96 -\\
97 -** [[image:attach:kamzik_tape.PNG||height="400"]]
97 +**Tape**
98 98  
99 +* Click on the 'main tape' icon
100 +* Change the velocity by typing anything from **0.3-3.0 mm/s**
101 +* Common velocity is 1.0-1.5 mm/s
102 +* kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
99 99  \\
104 +* [[image:attach:kamzik_tape.PNG||height="400"]]
100 100  
101 -* **Sample nozzle:**
102 -** Click an the 'nozzle' icon.
103 -** (((
106 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle:"/}}**Sample nozzle:** ====
107 +
108 +* Click an the 'nozzle' icon.
109 +* (((
104 104  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
105 105  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
106 106  \\(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%)
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150 150  **
151 151  \\**
152 152  )))
153 -** [[image:attach:kamzik_nozzle.PNG||height="400"]]
159 +* [[image:attach:kamzik_nozzle.PNG||height="400"]]
154 154  
161 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ====
162 +
155 155  \\
156 156  
157 157  \\
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158 158  
159 159  \\
160 160  
169 +\\
170 +
161 161  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
162 162  
163 163   xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611
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168 168  
169 169  \\
170 170  
171 -**14.5 Tape roll exchange**
181 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** ====
172 172  
173 173  The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s).
174 174  
Confluence.Code.ConfluencePageClass[0]
Id
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1 -235039461
1 +235039462
URL
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1 -https://confluence.desy.de/spaces/11/pages/235039461/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/235039462/14. Serial Crystallography: CFEL TapeDrive