Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
Summary
-
Page properties (1 modified, 0 added, 0 removed)
-
Objects (1 modified, 0 added, 0 removed)
Details
- Page properties
-
- Content
-
... ... @@ -1,5 +2,9 @@ 1 -[[image:attach:TapeDrive_beschriftet.PNG||height="400"]][[image:attach:TapeDrive scheme.png||height="400"]] 2 2 2 + 3 +{{toc/}} 4 + 5 +[[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 6 + 3 3 \\ 4 4 5 5 \\ ... ... @@ -75,14 +75,16 @@ 75 75 76 76 Be aware to which channel and nozzle line your sample is connected. 77 77 78 - Red → Channel 1, crystal line (nozzle capillary without marks) 82 + Red → Channel 1, crystal line (nozzle capillary without marks/with red marks) 79 79 80 80 Green → Channel 2, substrate line (nozzle capillary is marked in black) 81 81 82 82 [[image:attach:20211201_095033.jpg||thumbnail="true" height="250"]] 83 83 84 - \\88 +After finishing data collection, flush all lines by connecting an Eppi or syringe filled with ddH,,2,,O. 85 85 90 +[[image:attach:20211201_095232.jpg||height="250"]][[image:attach:20211201_095205.jpg||height="250"]] 91 + 86 86 \\ 87 87 88 88 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.4TapeDriveoperation"/}}**14.4 TapeDrive operation ... ... @@ -103,7 +103,7 @@ 103 103 \\ 104 104 * [[image:attach:kamzik_tape.PNG||height="400"]] 105 105 106 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle :"/}}**Sample nozzle:** ====112 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ==== 107 107 108 108 * Click an the 'nozzle' icon. 109 109 * ((( ... ... @@ -160,12 +160,16 @@ 160 160 161 161 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ==== 162 162 163 - \\169 +* The chiller circulates fluid through the gas nozzle. 164 164 165 165 \\ 166 166 173 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ==== 174 + 167 167 \\ 168 168 177 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}**IR camera** ==== 178 + 169 169 \\ 170 170 171 171 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: ... ... @@ -178,7 +178,7 @@ 178 178 179 179 \\ 180 180 181 -=== ={{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** ====191 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** === 182 182 183 183 The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s). 184 184 ... ... @@ -185,13 +185,14 @@ 185 185 * Remove the (almost) empty feeder roll by pulling it upwards. 186 186 * Cut the tape with some cm overlap to glue to the new roll. **Do not discard empty roll!** 187 187 * Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm** 188 -* Cut the first cm of the new tape roll, directly be forethe black sticky part.189 -* Usethis stickypart to attach the end of the old tape to thenewroll.Place new rollon roll holder.190 -* Open magnetic tape stabilizer. 191 -* Start the tape (3mm/s). Once the connetion side (black sticky part)has arrived at the collector roll, stop the tape (0mm/s).192 -* Again, cut the tape directly in frontof theblackmark. Replace the the old roll with the **empty **one. Old roll can be discarded.193 -* Attach new tape to the empty roll by using theblackstickypart.198 +* Cut the first cm of the new tape roll, directly behind the black sticky part. 199 +* Place new roll on roll holder and use sticky tape to attach the end of the old tape to the beginning of the new roll. 200 +* Open magnetic tape stabilizer on the **left side**. //!!!BEAMSTOP!!!// 201 +* Start the tape (3mm/s). Once the connetion side has arrived at the collector roll, stop the tape (0mm/s). 202 +* Again, cut the tape directly behind the connection side. Replace the the old roll with the **empty **one. Old roll can be discarded. 203 +* Attach new tape to the empty roll by using some sticky tape. 194 194 * Close tape stabilizer. 205 +* Reset tape counter in kamzik by clicking "<Call>" in "Main-Tape". 195 195 196 196 **[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]] 197 197 ** ... ... @@ -200,8 +200,26 @@ 200 200 201 201 \\ 202 202 214 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}14.6 Nozzle exchange === 215 + 203 203 \\ 204 204 218 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}14.7 Data collection === 219 + 205 205 \\ 206 206 222 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting === 223 + 224 +* ((( 225 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 226 +))) 227 +* ((( 228 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 229 +))) 230 +* ((( 231 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 232 +))) 233 + 207 207 \\ 235 + 236 +\\
- Confluence.Code.ConfluencePageClass[0]
-
- Id
-
... ... @@ -1,1 +1,1 @@ 1 -23 50394621 +236824561 - URL
-
... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/23 5039462/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824561/14. Serial Crystallography: CFEL TapeDrive