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Last modified by chatzies on 2025-11-27 11:35
From version 24.1
edited by ahenkel
on 2021-12-03 11:33
Change comment: There is no comment for this version
To version 22.1
edited by ahenkel
on 2021-12-03 11:26
Change comment: There is no comment for this version

Summary

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1 -
2 -
3 -{{toc/}}
4 -
5 5  [[image:attach:TapeDrive_beschriftet.PNG||height="400"]][[image:attach:TapeDrive scheme.png||height="400"]]
6 6  
7 -\\
3 +**14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)**
8 8  
9 -\\
10 -
11 -\\
12 -
13 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1RevertfromCrystallographytoTapeDrive(P11staff/CFEL)"/}}**14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)** ===
14 -
15 15  * remove vortex
16 16  * beamstop to out-position?
17 17  * remove goniometer. The airbearing should be stopped (p11/servermotor/eh.1.01)
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60 60  
61 61  \\
62 62  
63 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2Samplecharacteristicsandpreparation"/}}**14.2 Sample characteristics and preparation** ===
53 +**14.2 Sample characteristics and preparation**
64 64  
65 65  suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
66 66  
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72 72  
73 73  \\
74 74  
75 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3ConnectingsampletoElveFlow,sampleexchange"/}}**14.3 Connecting sample to ElveFlow, sample exchange
76 -** ===
65 +**14.3 Connecting sample to ElveFlow, sample exchange
66 +**
77 77  
78 78  After filtration, screw the ElveFlow connector to your Eppendorf or Falcon tube. Make sure that the yellow-ish line goes to the bottom of your tube. You can adjust the length by unscrewing the blue fitting on top and pushing/pulling the yellow-ish line. **Don't forget to tigthen the blue fitting afterwards!**
79 79  
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89 89  
90 90  \\
91 91  
92 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4TapeDriveoperation"/}}**14.4 TapeDrive operation
93 -** ===
82 +**14.4 TapeDrive operation
83 +**
94 94  
95 95  The TapeDrive is controlled through kamzik. To open kamzik, start the server. A terminal will open and shortly after a small window.
96 96  Now start the client. Same thing, a terminal will open, shortly after a small window.
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98 98  Click 'Devices' in the **client session** to open the control window.
99 99  [[image:attach:screen.PNG||height="250"]][[image:attach:server client.PNG||height="250"]]
100 100  
101 -**Tape**
91 +* **Tape:**
92 +** Click on the 'main tape' icon
93 +** Change the velocity by typing anything from **0.3-3.0 mm/s**
94 +** Common velocity is 1.0-1.5 mm/s
95 +** kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
96 +\\
97 +** [[image:attach:kamzik_tape.PNG||height="400"]]
102 102  
103 -* Click on the 'main tape' icon
104 -* Change the velocity by typing anything from **0.3-3.0 mm/s**
105 -* Common velocity is 1.0-1.5 mm/s
106 -* kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
107 107  \\
108 -* [[image:attach:kamzik_tape.PNG||height="400"]]
109 109  
110 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle:"/}}**Sample nozzle:** ====
111 -
112 -* Click an the 'nozzle' icon.
113 -* (((
101 +* **Sample nozzle:**
102 +** Click an the 'nozzle' icon.
103 +** (((
114 114  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
115 115  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
116 116  \\(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%)
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160 160  **
161 161  \\**
162 162  )))
163 -* [[image:attach:kamzik_nozzle.PNG||height="400"]]
153 +** [[image:attach:kamzik_nozzle.PNG||height="400"]]
164 164  
165 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ====
166 -
167 167  \\
168 168  
169 169  \\
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170 170  
171 171  \\
172 172  
173 -\\
174 -
175 175  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
176 176  
177 177   xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611
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182 182  
183 183  \\
184 184  
185 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** ====
171 +**14.5 Tape roll exchange**
186 186  
187 187  The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s).
188 188  
Confluence.Code.ConfluencePageClass[0]
Id
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1 -235039464
1 +235039461
URL
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1 -https://confluence.desy.de/spaces/11/pages/235039464/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/235039461/14. Serial Crystallography: CFEL TapeDrive