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Last modified by chatzies on 2025-11-27 11:35
From version 27.1
edited by ahenkel
on 2021-12-05 19:34
Change comment: There is no comment for this version
To version 35.1
edited by ahenkel
on 2021-12-12 22:09
Change comment: There is no comment for this version

Summary

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Content
... ... @@ -79,14 +79,16 @@
79 79  
80 80  Be aware to which channel and nozzle line your sample is connected.
81 81  
82 - Red → Channel 1, crystal line (nozzle capillary without marks)
82 + Red → Channel 1, crystal line (nozzle capillary without marks/with red marks)
83 83  
84 84   Green → Channel 2, substrate line (nozzle capillary is marked in black)
85 85  
86 86  [[image:attach:20211201_095033.jpg||thumbnail="true" height="250"]]
87 87  
88 -\\
88 +After finishing data collection, flush all lines by connecting an Eppi or syringe filled with ddH,,2,,O.
89 89  
90 +[[image:attach:20211201_095232.jpg||height="250"]][[image:attach:20211201_095205.jpg||height="250"]]
91 +
90 90  \\
91 91  
92 92  === {{id name="14.SerialCrystallography:CFELTapeDrive-14.4TapeDriveoperation"/}}**14.4 TapeDrive operation
... ... @@ -164,12 +164,16 @@
164 164  
165 165  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ====
166 166  
167 -\\
169 +* The chiller circulates fluid through the gas nozzle.
168 168  
169 169  \\
170 170  
173 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ====
174 +
171 171  \\
172 172  
177 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}**IR camera** ====
178 +
173 173  \\
174 174  
175 175  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
... ... @@ -189,13 +189,14 @@
189 189  * Remove the (almost) empty feeder roll by pulling it upwards.
190 190  * Cut the tape with some cm overlap to glue to the new roll. **Do not discard empty roll!**
191 191  * Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm**
192 -* Cut the first cm of the new tape roll, directly before the black sticky part.
193 -* Use this sticky part to attach the end of the old tape to the new roll. Place new roll on roll holder.
194 -* Open magnetic tape stabilizer.
195 -* Start the tape (3mm/s). Once the connetion side (black sticky part) has arrived at the collector roll, stop the tape (0mm/s).
196 -* Again, cut the tape directly in front of the black mark. Replace the the old roll with the **empty **one. Old roll can be discarded.
197 -* Attach new tape to the empty roll by using the black sticky part.
198 +* Cut the first cm of the new tape roll, directly behind the black sticky part.
199 +* Place new roll on roll holder and use sticky tape to attach the end of the old tape to the beginning of the new roll.
200 +* Open magnetic tape stabilizer on the **left side**. //!!!BEAMSTOP!!!//
201 +* Start the tape (3mm/s). Once the connetion side has arrived at the collector roll, stop the tape (0mm/s).
202 +* Again, cut the tape directly behind the connection side. Replace the the old roll with the **empty **one. Old roll can be discarded.
203 +* Attach new tape to the empty roll by using some sticky tape.
198 198  * Close tape stabilizer.
205 +* Reset tape counter in kamzik by clicking "<Call>" in "Main-Tape".
199 199  
200 200  **[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]]
201 201  **
... ... @@ -204,8 +204,26 @@
204 204  
205 205  \\
206 206  
214 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}14.6 Nozzle exchange ===
215 +
207 207  \\
208 208  
218 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}14.7 Data collection ===
219 +
209 209  \\
210 210  
222 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting ===
223 +
224 +* (((
225 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ====
226 +)))
227 +* (((
228 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ====
229 +)))
230 +* (((
231 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ====
232 +)))
233 +
211 211  \\
235 +
236 +\\
Confluence.Code.ConfluencePageClass[0]
Id
... ... @@ -1,1 +1,1 @@
1 -235041518
1 +236824561
URL
... ... @@ -1,1 +1,1 @@
1 -https://confluence.desy.de/spaces/11/pages/235041518/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/236824561/14. Serial Crystallography: CFEL TapeDrive