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Last modified by chatzies on 2025-11-27 11:35
From version 36.1
edited by ahenkel
on 2021-12-12 22:53
Change comment: There is no comment for this version
To version 35.1
edited by ahenkel
on 2021-12-12 22:09
Change comment: There is no comment for this version

Summary

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... ... @@ -115,11 +115,9 @@
115 115  * (((
116 116  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
117 117  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
118 +\\(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%)
119 +\\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments.
118 118  
119 -
120 -(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%)
121 -\\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments.
122 -
123 123  (% class="wrapped" %)
124 124  |=(((
125 125  \\
... ... @@ -206,7 +206,7 @@
206 206  * Close tape stabilizer.
207 207  * Reset tape counter in kamzik by clicking "<Call>" in "Main-Tape".
208 208  
209 -**[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]][[image:attach:tape reset.PNG||height="250"]]
207 +**[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]]
210 210  **
211 211  
212 212  \\
... ... @@ -213,130 +213,14 @@
213 213  
214 214  \\
215 215  
216 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** ===
214 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}14.6 Nozzle exchange ===
217 217  
218 218  \\
219 219  
220 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7 Data collection** ===
218 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}14.7 Data collection ===
221 221  
222 -Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
223 -
224 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611
225 - password: //written on control laptop (changes every 6 months)//
226 -
227 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
228 -
229 229  \\
230 230  
231 -**Check list:**
232 -
233 -* Open BS1  (//CrystalControl)//
234 -* Put collimator in (//CrystalControl)//
235 -* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)//
236 -* Open fast shutter (//CrystalControl)//
237 -* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)//
238 -* Close fast shutter (//CrystalControl)//
239 -
240 -\\
241 -
242 -**Start run in kamzik
243 -**
244 -
245 -Click "Start" icon in kamzik.
246 -
247 -[[image:attach:kamzik_run-tile.jpg||height="400"]]
248 -
249 -|=(((
250 -Parameter
251 -)))|=(((
252 -explanation
253 -)))|=(% colspan="1" %)(((
254 -value
255 -)))
256 -|(((
257 -Images number
258 -)))|(((
259 -Set number of frames you want to collect
260 -)))|(% colspan="1" %)(((
261 -usually 100k - 200k, but adjust according to hitrate
262 -
263 -orientation: 10 % hitrate needs at least 100k images
264 -)))
265 -|(((
266 -exposure
267 -)))|(((
268 -exposure time of Eiger
269 -
270 -\\
271 -)))|(% colspan="1" %)(((
272 -chopper at 133 Hz → 3.7 ms
273 -
274 -chopper at 66 Hz   → 7.7 ms
275 -
276 -no chopper            → 7.7 ms
277 -
278 -----
279 -)))
280 -|(((
281 -run id
282 -)))|(((
283 -changes automatically
284 -)))|(% colspan="1" %)(((
285 -\\
286 -)))
287 -|(% colspan="1" %)(((
288 -Detector distance
289 -)))|(% colspan="1" %)(((
290 -current detector postion readout
291 -)))|(% colspan="1" %)(((
292 -\\
293 -)))
294 -|(% colspan="1" %)(((
295 -move_detector (distance)
296 -)))|(% colspan="1" %)(((
297 -Set detector distance
298 -)))|(% colspan="1" %)(((
299 -200.0 mm   (% style="color: rgb(255,0,0);" %)confirm with //enter//, click "<Call>"
300 -)))
301 -|(% colspan="1" %)(((
302 -Diode voltage
303 -)))|(% colspan="1" %)(((
304 -read out of diode
305 -)))|(% colspan="1" %)(((
306 -**~~ 0 !!! higher values indicate missaligned beam stop!!!**
307 -)))
308 -
309 -----
310 -
311 -(% class="task-list" %)
312 -(((
313 -{{task reference="/Tasks/Task_6" status="InProgress"}}
314 -Set your desired No. of frames
315 -{{/task}}
316 -
317 -{{task reference="/Tasks/Task_7" status="InProgress"}}
318 -Match exposure time with chopper setting
319 -{{/task}}
320 -
321 -{{task reference="/Tasks/Task_8" status="InProgress"}}
322 -Check trigger setting and match to chopper setting
323 -{{/task}}
324 -
325 -{{task reference="/Tasks/Task_9" status="InProgress"}}
326 -Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it.
327 -{{/task}}
328 -
329 -{{task reference="/Tasks/Task_10" status="InProgress"}}
330 -To start the run, click "<Call>" next to //exposure time//
331 -{{/task}}
332 -)))
333 -
334 -----
335 -
336 -\\
337 -
338 -\\
339 -
340 340  === {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting ===
341 341  
342 342  * (((
Confluence.Code.ConfluencePageClass[0]
Id
... ... @@ -1,1 +1,1 @@
1 -236824562
1 +236824561
URL
... ... @@ -1,1 +1,1 @@
1 -https://confluence.desy.de/spaces/11/pages/236824562/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/236824561/14. Serial Crystallography: CFEL TapeDrive