Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,7 +1,6 @@ 1 - 2 - 3 -{{toc/}} 4 - 1 +{{layout}} 2 +{{layout-section ac:type="single"}} 3 +{{layout-cell}} 5 5 [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 6 6 7 7 \\ ... ... @@ -120,7 +120,6 @@ 120 120 (% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 121 121 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 122 122 123 -(% class="wrapped" %) 124 124 |=((( 125 125 \\ 126 126 )))|=((( ... ... @@ -214,22 +214,79 @@ 214 214 \\ 215 215 216 216 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** === 215 +{{/layout-cell}} 216 +{{/layout-section}} 217 217 218 -\\ 218 +{{layout-section ac:type="single"}} 219 +{{layout-cell}} 220 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 219 219 220 - === {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7Data collection** ===222 +start chopper gui from terminal: 221 221 224 +(% class="code" %) 225 +((( 226 + cd /gpfs/local/shared/ChopperControl 227 +))) 228 + 229 +(% class="code" %) 230 +((( 231 + python chopperControl.py 232 +))) 233 +{{/layout-cell}} 234 +{{/layout-section}} 235 + 236 +{{layout-section ac:type="two_equal"}} 237 +{{layout-cell}} 238 + [[image:attach:20211212_233140.jpg||height="250"]] 239 +{{/layout-cell}} 240 + 241 +{{layout-cell}} 242 +**Chopper → no Chopper** 243 + 244 +* decrease frequency by max. 10 Hz steps\\ 245 +** click arrow down 10x, "Set", arrow down 10x, "Set", .... 246 +* at frequency = 10 Hz, click "Stop" 247 +* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 248 + 249 +(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 250 + 251 +* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 252 +* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 253 +** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 254 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 255 +{{/layout-cell}} 256 +{{/layout-section}} 257 + 258 +{{layout-section ac:type="single"}} 259 +{{layout-cell}} 260 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 261 + 222 222 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 223 223 224 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 225 - password: //written on control laptop (changes every 6 months)// 264 +(% class="code" %) 265 +((( 266 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 267 + password: written on control laptop (changes every 6 months) 268 +))) 226 226 227 227 //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 228 228 229 229 \\ 230 230 274 +Click "Start" icon in kamzik. 275 + 276 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 277 + 278 +---- 279 +{{/layout-cell}} 280 +{{/layout-section}} 281 + 282 +{{layout-section ac:type="two_equal"}} 283 +{{layout-cell}} 231 231 **Check list:** 232 232 286 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 287 + 233 233 * Open BS1 (//CrystalControl)// 234 234 * Put collimator in (//CrystalControl)// 235 235 * Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// ... ... @@ -239,13 +239,33 @@ 239 239 240 240 \\ 241 241 242 -**Start run in kamzik 243 -** 297 +**Set run parameters and go 🏃💥** 244 244 245 -Click "Start" icon in kamzik. 299 +1. Set your desired No. of frames 300 +1. Match exposure time with chopper setting 301 +1. Check trigger setting and match to chopper setting 302 +1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 303 +1. To start the run, click "<Call>" next to //exposure time// 246 246 247 - [[image:attach:kamzik_run-tile.jpg||height="400"]]305 +\\ 248 248 307 +(% style="color: rgb(153,51,102);" %)**//Current bug~://** 308 + 309 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 310 + 311 + 312 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 313 + 314 +(% class="code" %) 315 +((( 316 + cd /gpfs/current/raw/scan_frames 317 + watch "ls -lrt <run number>/ | tail" 318 +\\\\\\\\ 319 +))) 320 +{{/layout-cell}} 321 + 322 +{{layout-cell}} 323 +(% class="wrapped relative-table" style="width: 100.0%;" %) 249 249 |=((( 250 250 Parameter 251 251 )))|=((( ... ... @@ -303,52 +303,45 @@ 303 303 )))|(% colspan="1" %)((( 304 304 read out of diode 305 305 )))|(% colspan="1" %)((( 306 -**~~ 0 !!! higher values indicate missaligned beam stop!!!** 381 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 382 +Call local contact 383 +** 307 307 ))) 385 +{{/layout-cell}} 386 +{{/layout-section}} 308 308 388 +{{layout-section ac:type="single"}} 389 +{{layout-cell}} 309 309 ---- 310 310 311 -(% class="task-list" %) 312 -((( 313 -{{task reference="/Tasks/Task_6" status="InProgress"}} 314 -Set your desired No. of frames 315 -{{/task}} 392 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 316 316 317 -{{task reference="/Tasks/Task_7" status="InProgress"}} 318 -Match exposure time with chopper setting 319 -{{/task}} 394 +* ((( 395 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 320 320 321 -{{task reference="/Tasks/Task_8" status="InProgress"}} 322 -Check trigger setting and match to chopper setting 323 -{{/task}} 324 - 325 -{{task reference="/Tasks/Task_9" status="InProgress"}} 326 -Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 327 -{{/task}} 328 - 329 -{{task reference="/Tasks/Task_10" status="InProgress"}} 330 -To start the run, click "<Call>" next to //exposure time// 331 -{{/task}} 397 +* Tape roll empty? 398 +* motor connected (icon green)? 332 332 ))) 333 333 334 ----- 335 - 336 336 \\ 337 337 338 -\\ 339 - 340 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting === 341 - 342 342 * ((( 343 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 344 -))) 345 -* ((( 346 346 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 405 + 406 +* displayed in green=connected? 407 +* nozzle holder colliding somewhere? 408 +* motor limits reached? → position displayed in red 347 347 ))) 348 -* ((( 349 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 350 -))) 351 351 352 352 \\ 353 353 354 -\\ 413 +* ((( 414 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 415 + 416 +* channel turned on? 417 +* Sample empty? 418 +* Nozzle or lines clogged? → flush with water, change nozzle 419 +))) 420 +{{/layout-cell}} 421 +{{/layout-section}} 422 +{{/layout}}
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... ... @@ -1,1 +1,1 @@ 1 -2368245 621 +236824590 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2368245 62/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824590/14. Serial Crystallography: CFEL TapeDrive