Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,10 +1,6 @@ 1 1 {{layout}} 2 2 {{layout-section ac:type="single"}} 3 3 {{layout-cell}} 4 - 5 - 6 -{{toc/}} 7 - 8 8 [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 9 9 10 10 \\ ... ... @@ -123,7 +123,6 @@ 123 123 (% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 124 124 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 125 125 126 -(% class="wrapped" %) 127 127 |=((( 128 128 \\ 129 129 )))|=((( ... ... @@ -217,22 +217,79 @@ 217 217 \\ 218 218 219 219 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** === 215 +{{/layout-cell}} 216 +{{/layout-section}} 220 220 221 -\\ 218 +{{layout-section ac:type="single"}} 219 +{{layout-cell}} 220 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 222 222 223 - === {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7Data collection** ===222 +start chopper gui from terminal: 224 224 224 +(% class="code" %) 225 +((( 226 + cd /gpfs/local/shared/ChopperControl 227 +))) 228 + 229 +(% class="code" %) 230 +((( 231 + python chopperControl.py 232 +))) 233 +{{/layout-cell}} 234 +{{/layout-section}} 235 + 236 +{{layout-section ac:type="two_equal"}} 237 +{{layout-cell}} 238 + [[image:attach:20211212_233140.jpg||height="250"]] 239 +{{/layout-cell}} 240 + 241 +{{layout-cell}} 242 +**Chopper → no Chopper** 243 + 244 +* decrease frequency by max. 10 Hz steps\\ 245 +** click arrow down 10x, "Set", arrow down 10x, "Set", .... 246 +* at frequency = 10 Hz, click "Stop" 247 +* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 248 + 249 +(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 250 + 251 +* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 252 +* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 253 +** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 254 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 255 +{{/layout-cell}} 256 +{{/layout-section}} 257 + 258 +{{layout-section ac:type="single"}} 259 +{{layout-cell}} 260 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 261 + 225 225 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 226 226 227 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 228 - password: //written on control laptop (changes every 6 months)// 264 +(% class="code" %) 265 +((( 266 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 267 + password: written on control laptop (changes every 6 months) 268 +))) 229 229 230 230 //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 231 231 232 232 \\ 233 233 274 +Click "Start" icon in kamzik. 275 + 276 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 277 + 278 +---- 279 +{{/layout-cell}} 280 +{{/layout-section}} 281 + 282 +{{layout-section ac:type="two_equal"}} 283 +{{layout-cell}} 234 234 **Check list:** 235 235 286 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 287 + 236 236 * Open BS1 (//CrystalControl)// 237 237 * Put collimator in (//CrystalControl)// 238 238 * Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// ... ... @@ -242,44 +242,33 @@ 242 242 243 243 \\ 244 244 245 -**Start run in kamzik 246 -** 297 +**Set run parameters and go 🏃💥** 247 247 248 -Click "Start" icon in kamzik. 299 +1. Set your desired No. of frames 300 +1. Match exposure time with chopper setting 301 +1. Check trigger setting and match to chopper setting 302 +1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 303 +1. To start the run, click "<Call>" next to //exposure time// 249 249 250 - [[image:attach:kamzik_run-tile.jpg||height="400"]]305 +\\ 251 251 252 ----- 253 -{{/layout-cell}} 254 -{{/layout-section}} 307 +(% style="color: rgb(153,51,102);" %)**//Current bug~://** 255 255 256 -{{layout-section ac:type="two_equal"}} 257 -{{layout-cell}} 258 -(% class="task-list" %) 259 -((( 260 -{{task reference="/Tasks/Task_16" status="InProgress"}} 261 -Set your desired No. of frames 262 -{{/task}} 309 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 263 263 264 -{{task reference="/Tasks/Task_17" status="InProgress"}} 265 -Match exposure time with chopper setting 266 -{{/task}} 267 267 268 -{{task reference="/Tasks/Task_18" status="InProgress"}} 269 -Check trigger setting and match to chopper setting 270 -{{/task}} 312 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 271 271 272 -{{task reference="/Tasks/Task_19" status="InProgress"}} 273 -Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 274 -{{/task}} 275 - 276 -{{task reference="/Tasks/Task_20" status="InProgress"}} 277 -To start the run, click "<Call>" next to //exposure time// 278 -{{/task}} 314 +(% class="code" %) 315 +((( 316 + cd /gpfs/current/raw/scan_frames 317 + watch "ls -lrt <run number>/ | tail" 318 +\\\\\\\\ 279 279 ))) 280 280 {{/layout-cell}} 281 281 282 282 {{layout-cell}} 323 +(% class="wrapped relative-table" style="width: 100.0%;" %) 283 283 |=((( 284 284 Parameter 285 285 )))|=((( ... ... @@ -337,7 +337,9 @@ 337 337 )))|(% colspan="1" %)((( 338 338 read out of diode 339 339 )))|(% colspan="1" %)((( 340 -**~~ 0 !!! higher values indicate missaligned beam stop!!!** 381 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 382 +Call local contact 383 +** 341 341 ))) 342 342 {{/layout-cell}} 343 343 {{/layout-section}} ... ... @@ -344,16 +344,35 @@ 344 344 345 345 {{layout-section ac:type="single"}} 346 346 {{layout-cell}} 347 - === {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting ===390 +---- 348 348 392 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 393 + 349 349 * ((( 350 350 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 396 + 397 +* Tape roll empty? 398 +* motor connected (icon green)? 351 351 ))) 400 + 401 +\\ 402 + 352 352 * ((( 353 353 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 405 + 406 +* displayed in green=connected? 407 +* nozzle holder colliding somewhere? 408 +* motor limits reached? → position displayed in red 354 354 ))) 410 + 411 +\\ 412 + 355 355 * ((( 356 356 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 415 + 416 +* channel turned on? 417 +* Sample empty? 418 +* Nozzle or lines clogged? → flush with water, change nozzle 357 357 ))) 358 358 {{/layout-cell}} 359 359 {{/layout-section}}
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... ... @@ -1,1 +1,1 @@ 1 -2368245 661 +236824590 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2368245 66/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824590/14. Serial Crystallography: CFEL TapeDrive