Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,10 +1,6 @@ 1 1 {{layout}} 2 2 {{layout-section ac:type="single"}} 3 3 {{layout-cell}} 4 - 5 - 6 -{{toc/}} 7 - 8 8 [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 9 9 10 10 \\ ... ... @@ -123,7 +123,6 @@ 123 123 (% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 124 124 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 125 125 126 -(% class="wrapped" %) 127 127 |=((( 128 128 \\ 129 129 )))|=((( ... ... @@ -217,34 +217,65 @@ 217 217 \\ 218 218 219 219 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** === 215 +{{/layout-cell}} 216 +{{/layout-section}} 220 220 221 -\\ 218 +{{layout-section ac:type="single"}} 219 +{{layout-cell}} 220 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 222 222 223 - === {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7Data collection** ===222 +start chopper gui from terminal: 224 224 225 -Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 224 +(% class="code" %) 225 +((( 226 + cd /gpfs/local/shared/ChopperControl 227 +))) 226 226 227 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 228 - password: //written on control laptop (changes every 6 months)// 229 +(% class="code" %) 230 +((( 231 + python chopperControl.py 232 +))) 233 +{{/layout-cell}} 234 +{{/layout-section}} 229 229 230 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 236 +{{layout-section ac:type="two_equal"}} 237 +{{layout-cell}} 238 + [[image:attach:20211212_233140.jpg||height="250"]] 239 +{{/layout-cell}} 231 231 232 -\\ 241 +{{layout-cell}} 242 +**Chopper → no Chopper** 233 233 234 -**Check list:** 244 +* decrease frequency by max. 10 Hz steps\\ 245 +** click arrow down 10x, "Set", arrow down 10x, "Set", .... 246 +* at frequency = 10 Hz, click "Stop" 247 +* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 235 235 236 -* Open BS1 (//CrystalControl)// 237 -* Put collimator in (//CrystalControl)// 238 -* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 239 -* Open fast shutter (//CrystalControl)// 240 -* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 241 -* Close fast shutter (//CrystalControl)// 249 +(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 242 242 243 -\\ 251 +* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 252 +* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 253 +** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 254 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 255 +{{/layout-cell}} 256 +{{/layout-section}} 244 244 245 -**Start run in kamzik 246 -** 258 +{{layout-section ac:type="single"}} 259 +{{layout-cell}} 260 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 247 247 262 +Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 263 + 264 +(% class="code" %) 265 +((( 266 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 267 + password: written on control laptop (changes every 6 months) 268 +))) 269 + 270 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 271 + 272 +\\ 273 + 248 248 Click "Start" icon in kamzik. 249 249 250 250 [[image:attach:kamzik_run-tile.jpg||height="400"]] ... ... @@ -255,17 +255,46 @@ 255 255 256 256 {{layout-section ac:type="two_equal"}} 257 257 {{layout-cell}} 284 +**Check list:** 285 + 286 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 287 + 288 +* Open BS1 (//CrystalControl)// 289 +* Put collimator in (//CrystalControl)// 290 +* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 291 +* Open fast shutter (//CrystalControl)// 292 +* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 293 +* Close fast shutter (//CrystalControl)// 294 + 258 258 \\ 259 259 297 +**Set run parameters and go 🏃💥** 298 + 260 260 1. Set your desired No. of frames 261 261 1. Match exposure time with chopper setting 262 262 1. Check trigger setting and match to chopper setting 263 263 1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 264 264 1. To start the run, click "<Call>" next to //exposure time// 304 + 305 +\\ 306 + 307 +(% style="color: rgb(153,51,102);" %)**//Current bug~://** 308 + 309 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 310 + 311 + 312 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 313 + 314 +(% class="code" %) 315 +((( 316 + cd /gpfs/current/raw/scan_frames 317 + watch "ls -lrt <run number>/ | tail" 318 +\\\\\\\\ 319 +))) 265 265 {{/layout-cell}} 266 266 267 267 {{layout-cell}} 268 -(% class="wrapped" %) 323 +(% class="wrapped relative-table" style="width: 100.0%;" %) 269 269 |=((( 270 270 Parameter 271 271 )))|=((( ... ... @@ -323,7 +323,9 @@ 323 323 )))|(% colspan="1" %)((( 324 324 read out of diode 325 325 )))|(% colspan="1" %)((( 326 -**~~ 0 !!! higher values indicate missaligned beam stop!!!** 381 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 382 +Call local contact 383 +** 327 327 ))) 328 328 {{/layout-cell}} 329 329 {{/layout-section}} ... ... @@ -330,16 +330,35 @@ 330 330 331 331 {{layout-section ac:type="single"}} 332 332 {{layout-cell}} 333 - === {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting ===390 +---- 334 334 392 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 393 + 335 335 * ((( 336 336 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 396 + 397 +* Tape roll empty? 398 +* motor connected (icon green)? 337 337 ))) 400 + 401 +\\ 402 + 338 338 * ((( 339 339 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 405 + 406 +* displayed in green=connected? 407 +* nozzle holder colliding somewhere? 408 +* motor limits reached? → position displayed in red 340 340 ))) 410 + 411 +\\ 412 + 341 341 * ((( 342 342 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 415 + 416 +* channel turned on? 417 +* Sample empty? 418 +* Nozzle or lines clogged? → flush with water, change nozzle 343 343 ))) 344 344 {{/layout-cell}} 345 345 {{/layout-section}}
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... ... @@ -1,1 +1,1 @@ 1 -2368245 731 +236824590 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2368245 73/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824590/14. Serial Crystallography: CFEL TapeDrive