Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,6 +1,7 @@ 1 -{{layout}} 2 -{{layout-section ac:type="single"}} 3 -{{layout-cell}} 1 + 2 + 3 +{{toc/}} 4 + 4 4 [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 5 5 6 6 \\ ... ... @@ -119,6 +119,7 @@ 119 119 (% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 120 120 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 121 121 123 +(% class="wrapped" %) 122 122 |=((( 123 123 \\ 124 124 )))|=((( ... ... @@ -212,79 +212,22 @@ 212 212 \\ 213 213 214 214 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** === 215 -{{/layout-cell}} 216 -{{/layout-section}} 217 217 218 -{{layout-section ac:type="single"}} 219 -{{layout-cell}} 220 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 218 +\\ 221 221 222 -star t chopperguifromterminal:220 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7 Data collection** === 223 223 224 -(% class="code" %) 225 -((( 226 - cd /gpfs/local/shared/ChopperControl 227 -))) 228 - 229 -(% class="code" %) 230 -((( 231 - python chopperControl.py 232 -))) 233 -{{/layout-cell}} 234 -{{/layout-section}} 235 - 236 -{{layout-section ac:type="two_equal"}} 237 -{{layout-cell}} 238 - [[image:attach:20211212_233140.jpg||height="250"]] 239 -{{/layout-cell}} 240 - 241 -{{layout-cell}} 242 -**Chopper → no Chopper** 243 - 244 -* decrease frequency by max. 10 Hz steps\\ 245 -** click arrow down 10x, "Set", arrow down 10x, "Set", .... 246 -* at frequency = 10 Hz, click "Stop" 247 -* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 248 - 249 -(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 250 - 251 -* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 252 -* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 253 -** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 254 -* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 255 -{{/layout-cell}} 256 -{{/layout-section}} 257 - 258 -{{layout-section ac:type="single"}} 259 -{{layout-cell}} 260 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 261 - 262 262 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 263 263 264 -(% class="code" %) 265 -((( 266 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 267 - password: written on control laptop (changes every 6 months) 268 -))) 224 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 225 + password: //written on control laptop (changes every 6 months)// 269 269 270 270 //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 271 271 272 272 \\ 273 273 274 -Click "Start" icon in kamzik. 275 - 276 -[[image:attach:kamzik_run-tile.jpg||height="400"]] 277 - 278 ----- 279 -{{/layout-cell}} 280 -{{/layout-section}} 281 - 282 -{{layout-section ac:type="two_equal"}} 283 -{{layout-cell}} 284 284 **Check list:** 285 285 286 -(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 287 - 288 288 * Open BS1 (//CrystalControl)// 289 289 * Put collimator in (//CrystalControl)// 290 290 * Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// ... ... @@ -294,33 +294,13 @@ 294 294 295 295 \\ 296 296 297 -**Set run parameters and go 🏃💥** 242 +**Start run in kamzik 243 +** 298 298 299 -1. Set your desired No. of frames 300 -1. Match exposure time with chopper setting 301 -1. Check trigger setting and match to chopper setting 302 -1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 303 -1. To start the run, click "<Call>" next to //exposure time// 245 +Click "Start" icon in kamzik. 304 304 305 - \\247 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 306 306 307 -(% style="color: rgb(153,51,102);" %)**//Current bug~://** 308 - 309 -(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 310 - 311 - 312 -(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 313 - 314 -(% class="code" %) 315 -((( 316 - cd /gpfs/current/raw/scan_frames 317 - watch "ls -lrt <run number>/ | tail" 318 -\\\\\\\\ 319 -))) 320 -{{/layout-cell}} 321 - 322 -{{layout-cell}} 323 -(% class="wrapped relative-table" style="width: 100.0%;" %) 324 324 |=((( 325 325 Parameter 326 326 )))|=((( ... ... @@ -378,45 +378,52 @@ 378 378 )))|(% colspan="1" %)((( 379 379 read out of diode 380 380 )))|(% colspan="1" %)((( 381 -**~~ 0 !!! higher values indicate missaligned beam stop!!! 382 -Call local contact 383 -** 306 +**~~ 0 !!! higher values indicate missaligned beam stop!!!** 384 384 ))) 385 -{{/layout-cell}} 386 -{{/layout-section}} 387 387 388 -{{layout-section ac:type="single"}} 389 -{{layout-cell}} 390 390 ---- 391 391 392 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 311 +(% class="task-list" %) 312 +((( 313 +{{task reference="/Tasks/Task_6" status="InProgress"}} 314 +Set your desired No. of frames 315 +{{/task}} 393 393 394 -* ((( 395 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 317 +{{task reference="/Tasks/Task_7" status="InProgress"}} 318 +Match exposure time with chopper setting 319 +{{/task}} 396 396 397 -* Tape roll empty? 398 -* motor connected (icon green)? 321 +{{task reference="/Tasks/Task_8" status="InProgress"}} 322 +Check trigger setting and match to chopper setting 323 +{{/task}} 324 + 325 +{{task reference="/Tasks/Task_9" status="InProgress"}} 326 +Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 327 +{{/task}} 328 + 329 +{{task reference="/Tasks/Task_10" status="InProgress"}} 330 +To start the run, click "<Call>" next to //exposure time// 331 +{{/task}} 399 399 ))) 400 400 334 +---- 335 + 401 401 \\ 402 402 338 +\\ 339 + 340 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting === 341 + 403 403 * ((( 343 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 344 +))) 345 +* ((( 404 404 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 405 - 406 -* displayed in green=connected? 407 -* nozzle holder colliding somewhere? 408 -* motor limits reached? → position displayed in red 409 409 ))) 410 - 411 -\\ 412 - 413 413 * ((( 414 414 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 415 - 416 -* channel turned on? 417 -* Sample empty? 418 -* Nozzle or lines clogged? → flush with water, change nozzle 419 419 ))) 420 -{{/layout-cell}} 421 -{{/layout-section}} 422 -{{/layout}} 351 + 352 +\\ 353 + 354 +\\
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... ... @@ -1,1 +1,1 @@ 1 -2368245 901 +236824562 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2368245 90/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824562/14. Serial Crystallography: CFEL TapeDrive