Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
Summary
-
Page properties (1 modified, 0 added, 0 removed)
-
Objects (1 modified, 0 added, 0 removed)
Details
- Page properties
-
- Content
-
... ... @@ -1,6 +1,10 @@ 1 1 {{layout}} 2 2 {{layout-section ac:type="single"}} 3 3 {{layout-cell}} 4 + 5 + 6 +{{toc/}} 7 + 4 4 [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 5 5 6 6 \\ ... ... @@ -119,6 +119,7 @@ 119 119 (% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 120 120 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 121 121 126 +(% class="wrapped" %) 122 122 |=((( 123 123 \\ 124 124 )))|=((( ... ... @@ -212,65 +212,34 @@ 212 212 \\ 213 213 214 214 === {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Nozzleexchange"/}}**14.6 Nozzle exchange** === 215 -{{/layout-cell}} 216 -{{/layout-section}} 217 217 218 -{{layout-section ac:type="single"}} 219 -{{layout-cell}} 220 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 221 +\\ 221 221 222 -star t chopperguifromterminal:223 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Datacollection"/}}**14.7 Data collection** === 223 223 224 -(% class="code" %) 225 -((( 226 - cd /gpfs/local/shared/ChopperControl 227 -))) 225 +Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 228 228 229 -(% class="code" %) 230 -((( 231 - python chopperControl.py 232 -))) 233 -{{/layout-cell}} 234 -{{/layout-section}} 227 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 228 + password: //written on control laptop (changes every 6 months)// 235 235 236 -{{layout-section ac:type="two_equal"}} 237 -{{layout-cell}} 238 - [[image:attach:20211212_233140.jpg||height="250"]] 239 -{{/layout-cell}} 230 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 240 240 241 -{{layout-cell}} 242 -**Chopper → no Chopper** 232 +\\ 243 243 244 -* decrease frequency by max. 10 Hz steps\\ 245 -** click arrow down 10x, "Set", arrow down 10x, "Set", .... 246 -* at frequency = 10 Hz, click "Stop" 247 -* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 234 +**Check list:** 248 248 249 -(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 236 +* Open BS1 (//CrystalControl)// 237 +* Put collimator in (//CrystalControl)// 238 +* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 239 +* Open fast shutter (//CrystalControl)// 240 +* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 241 +* Close fast shutter (//CrystalControl)// 250 250 251 -* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 252 -* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 253 -** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 254 -* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 255 -{{/layout-cell}} 256 -{{/layout-section}} 257 - 258 -{{layout-section ac:type="single"}} 259 -{{layout-cell}} 260 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 261 - 262 -Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 263 - 264 -(% class="code" %) 265 -((( 266 - xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 267 - password: written on control laptop (changes every 6 months) 268 -))) 269 - 270 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 271 - 272 272 \\ 273 273 245 +**Start run in kamzik 246 +** 247 + 274 274 Click "Start" icon in kamzik. 275 275 276 276 [[image:attach:kamzik_run-tile.jpg||height="400"]] ... ... @@ -281,46 +281,17 @@ 281 281 282 282 {{layout-section ac:type="two_equal"}} 283 283 {{layout-cell}} 284 -**Check list:** 285 - 286 -(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 287 - 288 -* Open BS1 (//CrystalControl)// 289 -* Put collimator in (//CrystalControl)// 290 -* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 291 -* Open fast shutter (//CrystalControl)// 292 -* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 293 -* Close fast shutter (//CrystalControl)// 294 - 295 295 \\ 296 296 297 -**Set run parameters and go 🏃💥** 298 - 299 299 1. Set your desired No. of frames 300 300 1. Match exposure time with chopper setting 301 301 1. Check trigger setting and match to chopper setting 302 302 1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 303 303 1. To start the run, click "<Call>" next to //exposure time// 304 - 305 -\\ 306 - 307 -(% style="color: rgb(153,51,102);" %)**//Current bug~://** 308 - 309 -(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 310 - 311 - 312 -(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 313 - 314 -(% class="code" %) 315 -((( 316 - cd /gpfs/current/raw/scan_frames 317 - watch "ls -lrt <run number>/ | tail" 318 -\\\\\\\\ 319 -))) 320 320 {{/layout-cell}} 321 321 322 322 {{layout-cell}} 323 -(% class="wrapped relative-table"style="width: 100.0%;" %)268 +(% class="wrapped" %) 324 324 |=((( 325 325 Parameter 326 326 )))|=((( ... ... @@ -378,9 +378,7 @@ 378 378 )))|(% colspan="1" %)((( 379 379 read out of diode 380 380 )))|(% colspan="1" %)((( 381 -**~~ 0 !!! higher values indicate missaligned beam stop!!! 382 -Call local contact 383 -** 326 +**~~ 0 !!! higher values indicate missaligned beam stop!!!** 384 384 ))) 385 385 {{/layout-cell}} 386 386 {{/layout-section}} ... ... @@ -387,35 +387,16 @@ 387 387 388 388 {{layout-section ac:type="single"}} 389 389 {{layout-cell}} 390 -- ---333 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Troubleshooting"/}}14.8 Troubleshooting === 391 391 392 -=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 393 - 394 394 * ((( 395 395 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 396 - 397 -* Tape roll empty? 398 -* motor connected (icon green)? 399 399 ))) 400 - 401 -\\ 402 - 403 403 * ((( 404 404 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 405 - 406 -* displayed in green=connected? 407 -* nozzle holder colliding somewhere? 408 -* motor limits reached? → position displayed in red 409 409 ))) 410 - 411 -\\ 412 - 413 413 * ((( 414 414 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 415 - 416 -* channel turned on? 417 -* Sample empty? 418 -* Nozzle or lines clogged? → flush with water, change nozzle 419 419 ))) 420 420 {{/layout-cell}} 421 421 {{/layout-section}}
- Confluence.Code.ConfluencePageClass[0]
-
- Id
-
... ... @@ -1,1 +1,1 @@ 1 -2368245 901 +236824573 - URL
-
... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2368245 90/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824573/14. Serial Crystallography: CFEL TapeDrive