Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
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... ... @@ -1,7 +1,7 @@ 1 1 {{layout}} 2 2 {{layout-section ac:type="single"}} 3 3 {{layout-cell}} 4 -[[image:attach:TapeDrive_beschriftet-tile.jpg||height=" 250"]]4 +[[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]] 5 5 6 6 \\ 7 7 ... ... @@ -9,6 +9,8 @@ 9 9 10 10 \\ 11 11 12 +---- 13 + 12 12 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** == 13 13 14 14 suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc. ... ... @@ -21,6 +21,8 @@ 21 21 22 22 \\ 23 23 26 +---- 27 + 24 24 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**14.2 Connecting sample to ElveFlow, sample exchange 25 25 ** == 26 26 ... ... @@ -40,6 +40,8 @@ 40 40 41 41 \\ 42 42 47 +---- 48 + 43 43 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**14.3 TapeDrive operation 44 44 ** == 45 45 ... ... @@ -139,8 +139,10 @@ 139 139 140 140 \\ 141 141 142 - == {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** ==148 +---- 143 143 150 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**14.4 Tape roll exchange** == 151 + 144 144 The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s). 145 145 146 146 * Remove the (almost) empty feeder roll by pulling it upwards. ... ... @@ -162,15 +162,17 @@ 162 162 163 163 \\ 164 164 165 - === {{id name="14.SerialCrystallography:CFELTapeDrive-"/}}**166 -** ===173 +** 174 +** 167 167 {{/layout-cell}} 168 168 {{/layout-section}} 169 169 170 170 {{layout-section ac:type="single"}} 171 171 {{layout-cell}} 172 - == {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** ==180 +---- 173 173 182 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**14.5 Chopper** == 183 + 174 174 start chopper gui from terminal: 175 175 176 176 (% class="code" %) ... ... @@ -181,6 +181,7 @@ 181 181 (% class="code" %) 182 182 ((( 183 183 python chopperControl.py 194 +\\\\ 184 184 ))) 185 185 {{/layout-cell}} 186 186 {{/layout-section}} ... ... @@ -207,9 +207,9 @@ 207 207 {{/layout-cell}} 208 208 {{/layout-section}} 209 209 210 -{{layout-section ac:type=" single"}}221 +{{layout-section ac:type="two_equal"}} 211 211 {{layout-cell}} 212 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14. 8Datacollection"/}}**14.8Data collection** ==223 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** == 213 213 214 214 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 215 215 ... ... @@ -219,33 +219,43 @@ 219 219 password: written on control laptop (changes every 6 months) 220 220 ))) 221 221 222 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//233 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 223 223 224 224 \\ 225 225 226 -C lick"Start"icon in kamzik.237 +**Check list:** 227 227 228 - [[image:attach:kamzik_run-tile.jpg||height="400"]]239 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 229 229 230 ----- 241 +(% style="color: rgb(0,0,0);" %)Click "Safety" icon in kamzik. 242 + 243 +* Put collimator in 244 +** Click "<Call>" next to //collimator_in// 245 + 246 +\\ 247 + 248 +* Open beam shutter BS1 in //CrystalControl// 231 231 {{/layout-cell}} 250 + 251 +{{layout-cell}} 252 +[[image:attach:kamzik_safety.PNG||height="400"]] 253 +{{/layout-cell}} 232 232 {{/layout-section}} 233 233 234 -{{layout-section ac:type=" two_equal"}}256 +{{layout-section ac:type="single"}} 235 235 {{layout-cell}} 236 - **Check list:**258 +---- 237 237 238 - (% style="color:rgb(255,0,0);"%)//always afterenteringthe hutch!//260 +Click "Start/Run" icon in kamzik. 239 239 240 -* Open BS1 (//CrystalControl)// 241 -* Put collimator in (//CrystalControl)// 242 -* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 243 -* Open fast shutter (//CrystalControl)// 244 -* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 245 -* Close fast shutter (//CrystalControl)// 262 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 246 246 247 -\\ 264 +---- 265 +{{/layout-cell}} 266 +{{/layout-section}} 248 248 268 +{{layout-section ac:type="two_equal"}} 269 +{{layout-cell}} 249 249 **Set run parameters and go 🏃💥** 250 250 251 251 1. Set your desired No. of frames ... ... @@ -256,19 +256,17 @@ 256 256 257 257 \\ 258 258 259 - (% style="color: rgb(153,51,102);" %)**//Current bug~://**280 +\\ 260 260 261 - (% style="color:rgb(0,0,0);" %)You needto "Stop" run in kamzikmanually after all images have been acquired. This movestheshield up andclosesthefast shutter.Afterwards youcan start a new run byclicking "<Call>".282 +**After data collection/Before entering the exp. hutch:** 262 262 284 +1. Go to "Safety" in kamzik. 285 +1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically: 286 +11. Drive the collimator out 287 +11. Drive the detector back to 1500 mm 288 +1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left). 263 263 264 -(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 265 - 266 -(% class="code" %) 267 -((( 268 - cd /gpfs/current/raw/scan_frames 269 - watch "ls -lrt <run number>/ | tail" 270 -\\\\\\\\ 271 -))) 290 +[[image:attach:Screenshot from 2022-04-04 19-36-29.png||height="400"]] 272 272 {{/layout-cell}} 273 273 274 274 {{layout-cell}} ... ... @@ -341,7 +341,7 @@ 341 341 {{layout-cell}} 342 342 ---- 343 343 344 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14. 9Troubleshooting"/}}**14.9Troubleshooting** ==363 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**14.7 Troubleshooting** == 345 345 346 346 * ((( 347 347 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== ... ... @@ -369,6 +369,41 @@ 369 369 * Sample empty? 370 370 * Nozzle or lines clogged? → flush with water, change nozzle 371 371 ))) 391 + 392 +\\ 393 + 394 +* ((( 395 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ==== 396 + 397 +* First, restart kamzik (server+client) and see if this solves the issue 398 +* If not, restart the Simplon server (in Astor → haspp11exp03, right click on Simplon/EH.1 and restart) 399 +* ((( 400 +If nothing works, kill the Simplon process and then start the server again:* ((( 401 +(% class="code" %) 402 +((( 403 +ssh haspp11exp03 404 +))) 405 +))) 406 +* ((( 407 +(% class="code" %) 408 +((( 409 +ps -ef | grep Simplon 410 +))) 411 +))) 412 +* ((( 413 +(% class="code" %) 414 +((( 415 +kill -9 simplon_process_id 416 +))) 417 +))) 418 +))) 419 +))) 372 372 {{/layout-cell}} 373 373 {{/layout-section}} 422 + 423 +{{layout-section ac:type="single"}} 424 +{{layout-cell}} 425 +\\ 426 +{{/layout-cell}} 427 +{{/layout-section}} 374 374 {{/layout}}
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... ... @@ -1,1 +1,1 @@ 1 -2 368245981 +250178642 - URL
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... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2 36824598/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/250178642/14. Serial Crystallography: CFEL TapeDrive