Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
Summary
-
Page properties (1 modified, 0 added, 0 removed)
-
Objects (1 modified, 0 added, 0 removed)
Details
- Page properties
-
- Content
-
... ... @@ -9,8 +9,6 @@ 9 9 10 10 \\ 11 11 12 ----- 13 - 14 14 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** == 15 15 16 16 suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc. ... ... @@ -23,8 +23,6 @@ 23 23 24 24 \\ 25 25 26 ----- 27 - 28 28 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**14.2 Connecting sample to ElveFlow, sample exchange 29 29 ** == 30 30 ... ... @@ -44,8 +44,6 @@ 44 44 45 45 \\ 46 46 47 ----- 48 - 49 49 == {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**14.3 TapeDrive operation 50 50 ** == 51 51 ... ... @@ -145,10 +145,8 @@ 145 145 146 146 \\ 147 147 148 -- ---142 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** == 149 149 150 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**14.4 Tape roll exchange** == 151 - 152 152 The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s). 153 153 154 154 * Remove the (almost) empty feeder roll by pulling it upwards. ... ... @@ -170,17 +170,15 @@ 170 170 171 171 \\ 172 172 173 -** 174 -** 165 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-"/}}** 166 +** === 175 175 {{/layout-cell}} 176 176 {{/layout-section}} 177 177 178 178 {{layout-section ac:type="single"}} 179 179 {{layout-cell}} 180 -- ---172 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** == 181 181 182 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**14.5 Chopper** == 183 - 184 184 start chopper gui from terminal: 185 185 186 186 (% class="code" %) ... ... @@ -191,7 +191,6 @@ 191 191 (% class="code" %) 192 192 ((( 193 193 python chopperControl.py 194 -\\\\ 195 195 ))) 196 196 {{/layout-cell}} 197 197 {{/layout-section}} ... ... @@ -218,9 +218,9 @@ 218 218 {{/layout-cell}} 219 219 {{/layout-section}} 220 220 221 -{{layout-section ac:type=" two_equal"}}210 +{{layout-section ac:type="single"}} 222 222 {{layout-cell}} 223 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14. 6Datacollection"/}}**14.6Data collection** ==212 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** == 224 224 225 225 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 226 226 ... ... @@ -230,43 +230,33 @@ 230 230 password: written on control laptop (changes every 6 months) 231 231 ))) 232 232 233 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 222 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 234 234 235 235 \\ 236 236 237 - **Checklist:**226 +Click "Start" icon in kamzik. 238 238 239 - (% style="color:rgb(255,0,0);" %)//alwaysafterenteringthehutch!//228 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 240 240 241 -(% style="color: rgb(0,0,0);" %)Click "Safety" icon in kamzik. 242 - 243 -* Put collimator in 244 -** Click "<Call>" next to //collimator_in// 245 - 246 -\\ 247 - 248 -* Open beam shutter BS1 in //CrystalControl// 230 +---- 249 249 {{/layout-cell}} 250 - 251 -{{layout-cell}} 252 -[[image:attach:kamzik_safety.PNG||height="400"]] 253 -{{/layout-cell}} 254 254 {{/layout-section}} 255 255 256 -{{layout-section ac:type=" single"}}234 +{{layout-section ac:type="two_equal"}} 257 257 {{layout-cell}} 258 - ----236 +**Check list:** 259 259 260 - Click"Start/Run"iconinkamzik.238 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 261 261 262 -[[image:attach:kamzik_run-tile.jpg||height="400"]] 240 +* Open BS1 (//CrystalControl)// 241 +* Put collimator in (//CrystalControl)// 242 +* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 243 +* Open fast shutter (//CrystalControl)// 244 +* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 245 +* Close fast shutter (//CrystalControl)// 263 263 264 ----- 265 -{{/layout-cell}} 266 -{{/layout-section}} 247 +\\ 267 267 268 -{{layout-section ac:type="two_equal"}} 269 -{{layout-cell}} 270 270 **Set run parameters and go 🏃💥** 271 271 272 272 1. Set your desired No. of frames ... ... @@ -277,17 +277,19 @@ 277 277 278 278 \\ 279 279 280 - \\259 +(% style="color: rgb(153,51,102);" %)**//Current bug~://** 281 281 282 - **After datacollection/before enteringthe exp.hutch**261 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 283 283 284 -1. Go to "Safety" in kamzik. 285 -1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically: 286 -11. Drive the collimator out 287 -11. Drive the detector back to 1500 mm 288 -1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left). 289 289 290 -[[image:attach:Screenshot from 2022-04-04 19-36-29.png||height="400"]] 264 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 265 + 266 +(% class="code" %) 267 +((( 268 + cd /gpfs/current/raw/scan_frames 269 + watch "ls -lrt <run number>/ | tail" 270 +\\\\\\\\ 271 +))) 291 291 {{/layout-cell}} 292 292 293 293 {{layout-cell}} ... ... @@ -360,7 +360,7 @@ 360 360 {{layout-cell}} 361 361 ---- 362 362 363 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14. 7Troubleshooting"/}}**14.7Troubleshooting** ==344 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}**14.9 Troubleshooting** == 364 364 365 365 * ((( 366 366 ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== ... ... @@ -388,41 +388,6 @@ 388 388 * Sample empty? 389 389 * Nozzle or lines clogged? → flush with water, change nozzle 390 390 ))) 391 - 392 -\\ 393 - 394 -* ((( 395 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ==== 396 - 397 -* First, restart kamzik (server+client) and see if this solves the issue 398 -* If not, restart the Simplon server (in Astor → haspp11exp03, right click on Simplon/EH.1 and restart) 399 -* ((( 400 -If nothing works, kill the Simplon process and then start the server again:* ((( 401 -(% class="code" %) 402 -((( 403 -ssh haspp11exp03 404 -))) 405 -))) 406 -* ((( 407 -(% class="code" %) 408 -((( 409 -ps -ef | grep Simplon 410 -))) 411 -))) 412 -* ((( 413 -(% class="code" %) 414 -((( 415 -kill -9 simplon_process_id 416 -))) 417 -))) 418 -))) 419 -))) 420 420 {{/layout-cell}} 421 421 {{/layout-section}} 422 - 423 -{{layout-section ac:type="single"}} 424 -{{layout-cell}} 425 -\\ 426 -{{/layout-cell}} 427 -{{/layout-section}} 428 428 {{/layout}}
- Confluence.Code.ConfluencePageClass[0]
-
- Id
-
... ... @@ -1,1 +1,1 @@ 1 -2 501786231 +236824598 - URL
-
... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/2 50178623/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824598/14. Serial Crystallography: CFEL TapeDrive