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Last modified by chatzies on 2025-11-27 11:35
From version 54.1
edited by ahenkel
on 2022-04-04 19:58
Change comment: There is no comment for this version
To version 60.1
edited by ahenkel
on 2022-04-14 11:58
Change comment: There is no comment for this version

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13 13  
14 14  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** ==
15 15  
16 -suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
16 +suspension of microcrystals, **at least** 200 µL with 20% crystal density (more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
17 17  
18 18  Preparation:
19 19  
20 -* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube
20 +* filter through 30 µm cell filter (green) or 50 µm (yellow) into Eppendorf or Falcon (original!) tube
21 21  
22 22  [[image:attach:20211201_095534.jpg||height="250"]]
23 23  
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156 156  * Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm**
157 157  * Cut the first cm of the new tape roll, directly behind the black sticky part.
158 158  * Place new roll on roll holder and use sticky tape to attach the end of the old tape to the beginning of the new roll.
159 -* Open magnetic tape stabilizer on the **left side**. //!!!BEAMSTOP!!!//
159 +* Open magnetic tape stabilizer on the **left side**. (% style="color: rgb(255,0,0);" %)//!!!BEAMSTOP!!!//
160 160  * Start the tape (3mm/s). Once the connetion side has arrived at the collector roll, stop the tape (0mm/s).
161 161  * Again, cut the tape directly behind the connection side. Replace the the old roll with the **empty **one. Old roll can be discarded.
162 162  * Attach new tape to the empty roll by using some sticky tape.
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218 218  {{/layout-cell}}
219 219  {{/layout-section}}
220 220  
221 -{{layout-section ac:type="two_equal"}}
221 +{{layout-section ac:type="single"}}
222 222  {{layout-cell}}
223 223  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
224 224  
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233 233   //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
234 234  
235 235  \\
236 +{{/layout-cell}}
237 +{{/layout-section}}
236 236  
239 +{{layout-section ac:type="two_left_sidebar"}}
240 +{{layout-cell}}
237 237  **Check list:**
238 238  
239 239  (% style="color: rgb(255,0,0);" %)//always after entering the hutch!//
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245 245  
246 246  \\
247 247  
248 -* Open beam shutter BS1 in //CrystalControl//
252 +* Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
249 249  {{/layout-cell}}
250 250  
251 251  {{layout-cell}}
Confluence.Code.ConfluencePageClass[0]
Id
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1 -250178642
1 +252820879
URL
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1 -https://confluence.desy.de/spaces/11/pages/250178642/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/252820879/14. Serial Crystallography: CFEL TapeDrive