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Last modified by chatzies on 2025-11-27 11:35
From version 58.1
edited by ahenkel
on 2022-04-04 20:02
Change comment: There is no comment for this version
To version 65.1
edited by ahenkel
on 2022-05-05 19:37
Change comment: There is no comment for this version

Summary

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... ... @@ -17,7 +17,7 @@
17 17  
18 18  Preparation:
19 19  
20 -* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube
20 +* filter through 30 µm cell filter (green) or 50 µm (yellow) into Eppendorf or Falcon (original!) tube
21 21  
22 22  [[image:attach:20211201_095534.jpg||height="250"]]
23 23  
... ... @@ -57,7 +57,7 @@
57 57  
58 58  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}**Tape** ====
59 59  
60 -* Click on the 'main tape' icon
60 +* Click the 'main tape' icon
61 61  * Change the velocity by typing anything from **0.3-3.0 mm/s**
62 62  * Common velocity is 1.0-1.5 mm/s
63 63  * kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
... ... @@ -66,7 +66,7 @@
66 66  
67 67  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ====
68 68  
69 -* Click an the 'nozzle' icon.
69 +* Click on the 'nozzle' icon.
70 70  * (((
71 71  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
72 72  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
... ... @@ -214,11 +214,12 @@
214 214  * (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes//
215 215  * (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps
216 216  ** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", .....
217 -* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms//
217 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms (technical exposure will always be 7.7 ms, since max. frame rate is 133 Hz
218 +//
218 218  {{/layout-cell}}
219 219  {{/layout-section}}
220 220  
221 -{{layout-section ac:type="two_right_sidebar"}}
222 +{{layout-section ac:type="single"}}
222 222  {{layout-cell}}
223 223  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
224 224  
... ... @@ -233,7 +233,11 @@
233 233   //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
234 234  
235 235  \\
237 +{{/layout-cell}}
238 +{{/layout-section}}
236 236  
240 +{{layout-section ac:type="two_left_sidebar"}}
241 +{{layout-cell}}
237 237  **Check list:**
238 238  
239 239  (% style="color: rgb(255,0,0);" %)//always after entering the hutch!//
... ... @@ -245,11 +245,11 @@
245 245  
246 246  \\
247 247  
248 -* Open beam shutter BS1 in //CrystalControl//
253 +* Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
249 249  {{/layout-cell}}
250 250  
251 251  {{layout-cell}}
252 -[[image:attach:kamzik_safety.PNG||height="250"]]
257 +[[image:attach:kamzik_safety.PNG||height="400"]]
253 253  {{/layout-cell}}
254 254  {{/layout-section}}
255 255  
... ... @@ -315,7 +315,7 @@
315 315  
316 316  \\
317 317  )))|(% colspan="1" %)(((
318 -chopper at 133 Hz → 3.7 ms
323 +chopper at 133 Hz → 7.7 ms (opening time will be 3.7)
319 319  
320 320  chopper at 66 Hz   → 7.7 ms
321 321  
... ... @@ -344,15 +344,6 @@
344 344  )))|(% colspan="1" %)(((
345 345  200.0 mm   (% style="color: rgb(255,0,0);" %)confirm with //enter//, click "<Call>"
346 346  )))
347 -|(% colspan="1" %)(((
348 -Diode voltage
349 -)))|(% colspan="1" %)(((
350 -read out of diode
351 -)))|(% colspan="1" %)(((
352 -**~~ 0 !!! higher values indicate missaligned beam stop!!! 
353 -Call local contact
354 -**
355 -)))
356 356  {{/layout-cell}}
357 357  {{/layout-section}}
358 358  
Confluence.Code.ConfluencePageClass[0]
Id
... ... @@ -1,1 +1,1 @@
1 -250178654
1 +254728507
URL
... ... @@ -1,1 +1,1 @@
1 -https://confluence.desy.de/spaces/11/pages/250178654/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/254728507/14. Serial Crystallography: CFEL TapeDrive