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Last modified by chatzies on 2025-11-27 11:35
From version 60.1
edited by ahenkel
on 2022-04-14 11:58
Change comment: There is no comment for this version
To version 49.1
edited by ahenkel
on 2022-04-04 14:43
Change comment: There is no comment for this version

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1 1  {{layout}}
2 2  {{layout-section ac:type="single"}}
3 3  {{layout-cell}}
4 -[[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]]
4 +[[image:attach:TapeDrive_beschriftet-tile.jpg||height="250"]]
5 5  
6 6  \\
7 7  
... ... @@ -13,11 +13,11 @@
13 13  
14 14  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** ==
15 15  
16 -suspension of microcrystals, **at least** 200 µL with 20% crystal density (more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
16 +suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
17 17  
18 18  Preparation:
19 19  
20 -* filter through 30 µm cell filter (green) or 50 µm (yellow) into Eppendorf or Falcon (original!) tube
20 +* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube
21 21  
22 22  [[image:attach:20211201_095534.jpg||height="250"]]
23 23  
... ... @@ -156,7 +156,7 @@
156 156  * Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm**
157 157  * Cut the first cm of the new tape roll, directly behind the black sticky part.
158 158  * Place new roll on roll holder and use sticky tape to attach the end of the old tape to the beginning of the new roll.
159 -* Open magnetic tape stabilizer on the **left side**. (% style="color: rgb(255,0,0);" %)//!!!BEAMSTOP!!!//
159 +* Open magnetic tape stabilizer on the **left side**. //!!!BEAMSTOP!!!//
160 160  * Start the tape (3mm/s). Once the connetion side has arrived at the collector roll, stop the tape (0mm/s).
161 161  * Again, cut the tape directly behind the connection side. Replace the the old roll with the **empty **one. Old roll can be discarded.
162 162  * Attach new tape to the empty roll by using some sticky tape.
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220 220  
221 221  {{layout-section ac:type="single"}}
222 222  {{layout-cell}}
223 +----
224 +
223 223  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
224 224  
225 225  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
... ... @@ -230,47 +230,33 @@
230 230   password: written on control laptop (changes every 6 months)
231 231  )))
232 232  
233 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
235 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
234 234  
235 235  \\
238 +
239 +Click "Start" icon in kamzik.
240 +
241 +[[image:attach:kamzik_run-tile.jpg||height="400"]]
242 +
243 +----
236 236  {{/layout-cell}}
237 237  {{/layout-section}}
238 238  
239 -{{layout-section ac:type="two_left_sidebar"}}
247 +{{layout-section ac:type="two_equal"}}
240 240  {{layout-cell}}
241 241  **Check list:**
242 242  
243 243  (% style="color: rgb(255,0,0);" %)//always after entering the hutch!//
244 244  
245 -(% style="color: rgb(0,0,0);" %)Click "Safety" icon in kamzik.
253 +* Open BS1  (//CrystalControl)//
254 +* Put collimator in (//CrystalControl)//
255 +* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)//
256 +* Open fast shutter (//CrystalControl)//
257 +* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)//
258 +* Close fast shutter (//CrystalControl)//
246 246  
247 -* Put collimator in
248 -** Click "<Call>" next to //collimator_in//
249 -
250 250  \\
251 251  
252 -* Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
253 -{{/layout-cell}}
254 -
255 -{{layout-cell}}
256 -[[image:attach:kamzik_safety.PNG||height="400"]]
257 -{{/layout-cell}}
258 -{{/layout-section}}
259 -
260 -{{layout-section ac:type="single"}}
261 -{{layout-cell}}
262 -----
263 -
264 -Click "Start/Run" icon in kamzik.
265 -
266 -[[image:attach:kamzik_run-tile.jpg||height="400"]]
267 -
268 -----
269 -{{/layout-cell}}
270 -{{/layout-section}}
271 -
272 -{{layout-section ac:type="two_equal"}}
273 -{{layout-cell}}
274 274  **Set run parameters and go 🏃💥**
275 275  
276 276  1. Set your desired No. of frames
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281 281  
282 282  \\
283 283  
284 -\\
272 +(% style="color: rgb(153,51,102);" %)**//Current bug~://**
285 285  
286 -**After data collection/Before entering the exp. hutch:**
274 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>".
287 287  
288 -1. Go to "Safety" in kamzik.
289 -1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically:
290 -11. Drive the collimator out
291 -11. Drive the detector back to 1500 mm
292 -1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left).
293 293  
294 -[[image:attach:Screenshot from 2022-04-04 19-36-29.png||height="400"]]
277 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with:
278 +
279 +(% class="code" %)
280 +(((
281 + cd /gpfs/current/raw/scan_frames
282 + watch "ls -lrt <run number>/ | tail"
283 +\\\\\\\\
284 +)))
295 295  {{/layout-cell}}
296 296  
297 297  {{layout-cell}}
... ... @@ -392,41 +392,16 @@
392 392  * Sample empty?
393 393  * Nozzle or lines clogged? → flush with water, change nozzle
394 394  )))
395 -
396 -\\
397 -
398 398  * (((
399 399  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ====
400 400  
401 401  * First, restart kamzik (server+client) and see if this solves the issue
402 402  * If not, restart the Simplon server (in Astor → haspp11exp03, right click on Simplon/EH.1 and restart)
403 -* (((
404 -If nothing works, kill the Simplon process and then start the server again:* (((
405 -(% class="code" %)
406 -(((
407 -ssh haspp11exp03
390 +* If nothing works, kill the Simplon process and then start the server again:
391 +** ssh haspp11exp03
392 +** ps -ef | grep Simplon
393 +** kill -9 simplon_process_id
408 408  )))
409 -)))
410 -* (((
411 -(% class="code" %)
412 -(((
413 -ps -ef | grep Simplon
414 -)))
415 -)))
416 -* (((
417 -(% class="code" %)
418 -(((
419 -kill -9 simplon_process_id
420 -)))
421 -)))
422 -)))
423 -)))
424 424  {{/layout-cell}}
425 425  {{/layout-section}}
426 -
427 -{{layout-section ac:type="single"}}
428 -{{layout-cell}}
429 -\\
430 -{{/layout-cell}}
431 -{{/layout-section}}
432 432  {{/layout}}
Confluence.Code.ConfluencePageClass[0]
Id
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1 -252820879
1 +250178591
URL
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1 -https://confluence.desy.de/spaces/11/pages/252820879/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/250178591/14. Serial Crystallography: CFEL TapeDrive