Skip to Content
Last modified by chatzies on 2025-11-27 11:35
From version 65.1
edited by ahenkel
on 2022-05-05 19:37
Change comment: There is no comment for this version
To version 57.1
edited by ahenkel
on 2022-04-04 20:01
Change comment: There is no comment for this version

Summary

Details

Page properties
Content
... ... @@ -17,7 +17,7 @@
17 17  
18 18  Preparation:
19 19  
20 -* filter through 30 µm cell filter (green) or 50 µm (yellow) into Eppendorf or Falcon (original!) tube
20 +* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube
21 21  
22 22  [[image:attach:20211201_095534.jpg||height="250"]]
23 23  
... ... @@ -57,7 +57,7 @@
57 57  
58 58  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}**Tape** ====
59 59  
60 -* Click the 'main tape' icon
60 +* Click on the 'main tape' icon
61 61  * Change the velocity by typing anything from **0.3-3.0 mm/s**
62 62  * Common velocity is 1.0-1.5 mm/s
63 63  * kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
... ... @@ -66,7 +66,7 @@
66 66  
67 67  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ====
68 68  
69 -* Click on the 'nozzle' icon.
69 +* Click an the 'nozzle' icon.
70 70  * (((
71 71  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
72 72  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
... ... @@ -214,12 +214,11 @@
214 214  * (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes//
215 215  * (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps
216 216  ** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", .....
217 -* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms (technical exposure will always be 7.7 ms, since max. frame rate is 133 Hz
218 -//
217 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms//
219 219  {{/layout-cell}}
220 220  {{/layout-section}}
221 221  
222 -{{layout-section ac:type="single"}}
221 +{{layout-section ac:type="two_equal"}}
223 223  {{layout-cell}}
224 224  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
225 225  
... ... @@ -234,11 +234,7 @@
234 234   //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
235 235  
236 236  \\
237 -{{/layout-cell}}
238 -{{/layout-section}}
239 239  
240 -{{layout-section ac:type="two_left_sidebar"}}
241 -{{layout-cell}}
242 242  **Check list:**
243 243  
244 244  (% style="color: rgb(255,0,0);" %)//always after entering the hutch!//
... ... @@ -250,11 +250,11 @@
250 250  
251 251  \\
252 252  
253 -* Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
248 +* Open beam shutter BS1 in //CrystalControl//
254 254  {{/layout-cell}}
255 255  
256 256  {{layout-cell}}
257 -[[image:attach:kamzik_safety.PNG||height="400"]]
252 +[[image:attach:kamzik_safety.PNG||height="250"]]
258 258  {{/layout-cell}}
259 259  {{/layout-section}}
260 260  
... ... @@ -320,7 +320,7 @@
320 320  
321 321  \\
322 322  )))|(% colspan="1" %)(((
323 -chopper at 133 Hz → 7.7 ms (opening time will be 3.7)
318 +chopper at 133 Hz → 3.7 ms
324 324  
325 325  chopper at 66 Hz   → 7.7 ms
326 326  
... ... @@ -349,6 +349,15 @@
349 349  )))|(% colspan="1" %)(((
350 350  200.0 mm   (% style="color: rgb(255,0,0);" %)confirm with //enter//, click "<Call>"
351 351  )))
347 +|(% colspan="1" %)(((
348 +Diode voltage
349 +)))|(% colspan="1" %)(((
350 +read out of diode
351 +)))|(% colspan="1" %)(((
352 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 
353 +Call local contact
354 +**
355 +)))
352 352  {{/layout-cell}}
353 353  {{/layout-section}}
354 354  
Confluence.Code.ConfluencePageClass[0]
Id
... ... @@ -1,1 +1,1 @@
1 -254728507
1 +250178651
URL
... ... @@ -1,1 +1,1 @@
1 -https://confluence.desy.de/spaces/11/pages/254728507/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/250178651/14. Serial Crystallography: CFEL TapeDrive