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Last modified by chatzies on 2025-11-27 11:35
From version 68.1
edited by ahenkel
on 2022-05-07 18:53
Change comment: There is no comment for this version
To version 58.1
edited by ahenkel
on 2022-04-04 20:02
Change comment: There is no comment for this version

Summary

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... ... @@ -17,7 +17,7 @@
17 17  
18 18  Preparation:
19 19  
20 -* filter through 30 µm cell filter (green) or 50 µm (yellow) into Eppendorf or Falcon (original!) tube
20 +* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube
21 21  
22 22  [[image:attach:20211201_095534.jpg||height="250"]]
23 23  
... ... @@ -57,7 +57,7 @@
57 57  
58 58  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}**Tape** ====
59 59  
60 -* Click the 'main tape' icon
60 +* Click on the 'main tape' icon
61 61  * Change the velocity by typing anything from **0.3-3.0 mm/s**
62 62  * Common velocity is 1.0-1.5 mm/s
63 63  * kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point.
... ... @@ -66,7 +66,7 @@
66 66  
67 67  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ====
68 68  
69 -* Click on the 'nozzle' icon.
69 +* Click an the 'nozzle' icon.
70 70  * (((
71 71  The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully.
72 72  The absolute position is **not calibrated** and therefore changes after each restart of kamzik.
... ... @@ -214,12 +214,11 @@
214 214  * (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes//
215 215  * (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps
216 216  ** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", .....
217 -* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms (technical exposure will always be 7.7 ms, since max. frame rate is 133 Hz
218 -//
217 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms//
219 219  {{/layout-cell}}
220 220  {{/layout-section}}
221 221  
222 -{{layout-section ac:type="single"}}
221 +{{layout-section ac:type="two_right_sidebar"}}
223 223  {{layout-cell}}
224 224  == {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
225 225  
... ... @@ -234,44 +234,65 @@
234 234   //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password//
235 235  
236 236  \\
237 -{{/layout-cell}}
238 -{{/layout-section}}
239 239  
240 -{{layout-section ac:type="two_left_sidebar"}}
241 -{{layout-cell}}
242 242  **Check list:**
243 243  
244 244  (% style="color: rgb(255,0,0);" %)//always after entering the hutch!//
245 245  
246 -(% style="color: rgb(0,0,0);" %)Click "Run" icon in kamzik.
241 +(% style="color: rgb(0,0,0);" %)Click "Safety" icon in kamzik.
247 247  
248 248  * Put collimator in
249 -** Put detector distance 200 in //prepare_for_measurement (      )
250 -//
251 -** Click "<Call>" next to //prepare_for_measurement//
244 +** Click "<Call>" next to //collimator_in//
252 252  
253 253  \\
254 254  
255 -* Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
248 +* Open beam shutter BS1 in //CrystalControl//
249 +{{/layout-cell}}
256 256  
257 -\\
258 -
259 -//**Set run parameters and go 🏃💥**//
260 -
261 -1. Set your desired No. of frames
262 -1. Match exposure time with chopper setting or set desired exposure time
263 -1. Check trigger setting and match to chopper setting
264 -1. To start the run, click "<Call>" next to //start_run (exposure    )//
251 +{{layout-cell}}
252 +[[image:attach:kamzik_safety.PNG||height="250"]]
265 265  {{/layout-cell}}
254 +{{/layout-section}}
266 266  
256 +{{layout-section ac:type="single"}}
267 267  {{layout-cell}}
268 -[[image:attach:Kamzik_run(2).PNG||height="400"]]
258 +----
259 +
260 +Click "Start/Run" icon in kamzik.
261 +
262 +[[image:attach:kamzik_run-tile.jpg||height="400"]]
263 +
264 +----
269 269  {{/layout-cell}}
270 270  {{/layout-section}}
271 271  
272 272  {{layout-section ac:type="two_equal"}}
273 273  {{layout-cell}}
274 -(% class="relative-table" %)
270 +**Set run parameters and go 🏃💥**
271 +
272 +1. Set your desired No. of frames
273 +1. Match exposure time with chopper setting
274 +1. Check trigger setting and match to chopper setting
275 +1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it.
276 +1. To start the run, click "<Call>" next to //exposure time//
277 +
278 +\\
279 +
280 +\\
281 +
282 +**After data collection/Before entering the exp. hutch:**
283 +
284 +1. Go to "Safety" in kamzik.
285 +1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically:
286 +11. Drive the collimator out
287 +11. Drive the detector back to 1500 mm
288 +1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left).
289 +
290 +[[image:attach:Screenshot from 2022-04-04 19-36-29.png||height="400"]]
291 +{{/layout-cell}}
292 +
293 +{{layout-cell}}
294 +(% class="wrapped relative-table" style="width: 100.0%;" %)
275 275  |=(((
276 276  Parameter
277 277  )))|=(((
... ... @@ -295,7 +295,7 @@
295 295  
296 296  \\
297 297  )))|(% colspan="1" %)(((
298 -chopper at 133 Hz → 7.7 ms (opening time will be 3.7)
318 +chopper at 133 Hz → 3.7 ms
299 299  
300 300  chopper at 66 Hz   → 7.7 ms
301 301  
... ... @@ -324,19 +324,16 @@
324 324  )))|(% colspan="1" %)(((
325 325  200.0 mm   (% style="color: rgb(255,0,0);" %)confirm with //enter//, click "<Call>"
326 326  )))
347 +|(% colspan="1" %)(((
348 +Diode voltage
349 +)))|(% colspan="1" %)(((
350 +read out of diode
351 +)))|(% colspan="1" %)(((
352 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 
353 +Call local contact
354 +**
355 +)))
327 327  {{/layout-cell}}
328 -
329 -{{layout-cell}}
330 -**After data collection/Before entering the exp. hutch:**
331 -
332 -1. Go to "Safety" in kamzik.
333 -1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically:
334 -11. Drive the collimator out
335 -11. Drive the detector back to 1500 mm
336 -1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left).
337 -
338 -[[image:attach:Screenshot from 2022-04-04 19-36-29.png||height="400"]]
339 -{{/layout-cell}}
340 340  {{/layout-section}}
341 341  
342 342  {{layout-section ac:type="single"}}
Confluence.Code.ConfluencePageClass[0]
Id
... ... @@ -1,1 +1,1 @@
1 -254729370
1 +250178654
URL
... ... @@ -1,1 +1,1 @@
1 -https://confluence.desy.de/spaces/11/pages/254729370/14. Serial Crystallography: CFEL TapeDrive
1 +https://confluence.desy.de/spaces/11/pages/250178654/14. Serial Crystallography: CFEL TapeDrive