Skip to Content
Last modified by chatzies on 2025-11-27 11:35
From version 77.1
edited by tabermah
on 2024-12-03 11:26
Change comment: There is no comment for this version
To version 79.1
edited by tabermah
on 2024-12-03 11:38
Change comment: There is no comment for this version

Summary

Details

Page properties
Title
... ... @@ -1,1 +1,1 @@
1 -10. Serial Crystallography: CFEL TapeDrive
1 +08. Serial Crystallography: CFEL TapeDrive
Content
... ... @@ -9,7 +9,7 @@
9 9  
10 10  ----
11 11  
12 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** ==
12 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**8.1 Sample characteristics and preparation** ==
13 13  
14 14  suspension of microcrystals, **at least** 200 µL with 20% crystal density (more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
15 15  
... ... @@ -22,7 +22,7 @@
22 22  
23 23  ----
24 24  
25 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**14.2 Connecting sample to ElveFlow, sample exchange** ==
25 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**8.2 Connecting sample to ElveFlow, sample exchange** ==
26 26  
27 27  *
28 28  ** ==
... ... @@ -44,7 +44,7 @@
44 44  
45 45  ----
46 46  
47 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**14.3 TapeDrive operation** ==
47 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**8.3 TapeDrive operation** ==
48 48  
49 49  *
50 50  ** ==
... ... @@ -116,7 +116,6 @@
116 116  be careful with -z, tape could be pushed out of focus
117 117  )))
118 118  
119 -
120 120  
121 121  )))
122 122  * [[image:attach:kamzik_nozzle.PNG||height="400"]]
... ... @@ -125,7 +125,6 @@
125 125  
126 126  * The chiller circulates fluid through the gas nozzle.
127 127  
128 -
129 129  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ====
130 130  
131 131  
... ... @@ -141,7 +141,7 @@
141 141  
142 142  ----
143 143  
144 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**14.4 Tape roll exchange** ==
142 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**8.4 Tape roll exchange** ==
145 145  
146 146  The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s).
147 147  
... ... @@ -169,7 +169,7 @@
169 169  {{layout-cell}}
170 170  ----
171 171  
172 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**14.5 Chopper** ==
170 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**8.5 Chopper** ==
173 173  
174 174  start chopper gui from terminal:
175 175  
... ... @@ -212,7 +212,7 @@
212 212  {{layout-cell}}
213 213  ----
214 214  
215 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
213 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**8.6 Data collection** ==
216 216  
217 217  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
218 218  
... ... @@ -242,10 +242,8 @@
242 242  ** drive the collimator in //IN// position
243 243  ** drive detector to 200 mm
244 244  
245 -
246 246  * Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
247 247  
248 -
249 249  //**Set run parameters and go 🏃💥**//
250 250  
251 251  1. Set your desired No. of frames
... ... @@ -347,7 +347,7 @@
347 347  {{layout-cell}}
348 348  ----
349 349  
350 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**14.7 Troubleshooting** ==
346 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**8.7 Troubleshooting** ==
351 351  
352 352  * (((
353 353  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ====
... ... @@ -356,7 +356,6 @@
356 356  * motor connected (icon green)?
357 357  )))
358 358  
359 -
360 360  * (((
361 361  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ====
362 362  
... ... @@ -365,7 +365,6 @@
365 365  * motor limits reached? → position displayed in red
366 366  )))
367 367  
368 -
369 369  * (((
370 370  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ====
371 371  
... ... @@ -374,7 +374,6 @@
374 374  * Nozzle or lines clogged? → flush with water, change nozzle
375 375  )))
376 376  
377 -
378 378  * (((
379 379  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ====
380 380