Skip to Content
Last modified by chatzies on 2025-11-27 11:35
From version 77.1
edited by tabermah
on 2024-12-03 11:26
Change comment: There is no comment for this version
To version 79.5
edited by tabermah
on 2024-12-10 15:19
Change comment: There is no comment for this version

Summary

Details

Page properties
Title
... ... @@ -1,1 +1,1 @@
1 -10. Serial Crystallography: CFEL TapeDrive
1 +08. Serial Crystallography: CFEL TapeDrive
Content
... ... @@ -4,12 +4,12 @@
4 4  [[image:attach:TapeDrive_beschriftet-tile.jpg||height="400"]]
5 5  
6 6  
7 -{{toc minLevel="2"/}}
7 +{{toc/}}
8 8  
9 9  
10 10  ----
11 11  
12 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** ==
12 += {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}8.1 Sample characteristics and preparation =
13 13  
14 14  suspension of microcrystals, **at least** 200 µL with 20% crystal density (more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
15 15  
... ... @@ -22,7 +22,7 @@
22 22  
23 23  ----
24 24  
25 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**14.2 Connecting sample to ElveFlow, sample exchange** ==
25 += {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}8.2 Connecting sample to ElveFlow, sample exchange =
26 26  
27 27  *
28 28  ** ==
... ... @@ -44,7 +44,7 @@
44 44  
45 45  ----
46 46  
47 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**14.3 TapeDrive operation** ==
47 += {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}8.3 TapeDrive operation =
48 48  
49 49  *
50 50  ** ==
... ... @@ -55,7 +55,7 @@
55 55  Click 'Devices' in the **client session** to open the control window.
56 56  [[image:attach:screen.PNG||height="250"]][[image:attach:server client.PNG||height="250"]]
57 57  
58 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}**Tape** ====
58 +== {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}Tape ==
59 59  
60 60  * Click the 'main tape' icon
61 61  * Change the velocity by typing anything from **0.3-3.0 mm/s**
... ... @@ -64,7 +64,7 @@
64 64  
65 65  * [[image:attach:kamzik_tape.PNG||height="400"]]
66 66  
67 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ====
67 +== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}Sample nozzle ==
68 68  
69 69  * Click on the 'nozzle' icon.
70 70  * (((
... ... @@ -116,22 +116,20 @@
116 116  be careful with -z, tape could be pushed out of focus
117 117  )))
118 118  
119 -
120 120  
121 121  )))
122 122  * [[image:attach:kamzik_nozzle.PNG||height="400"]]
123 123  
124 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ====
123 +== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}Temperature control/Chiller ==
125 125  
126 126  * The chiller circulates fluid through the gas nozzle.
127 127  
127 +== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}Gas nozzle ==
128 128  
129 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ====
130 130  
130 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}IR camera ====
131 131  
132 -==== {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}**IR camera** ====
133 133  
134 -
135 135  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
136 136  
137 137   xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611
... ... @@ -141,7 +141,7 @@
141 141  
142 142  ----
143 143  
144 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**14.4 Tape roll exchange** ==
142 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**8.4 Tape roll exchange** ==
145 145  
146 146  The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s).
147 147  
... ... @@ -169,7 +169,7 @@
169 169  {{layout-cell}}
170 170  ----
171 171  
172 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**14.5 Chopper** ==
170 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**8.5 Chopper** ==
173 173  
174 174  start chopper gui from terminal:
175 175  
... ... @@ -212,7 +212,7 @@
212 212  {{layout-cell}}
213 213  ----
214 214  
215 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
213 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**8.6 Data collection** ==
216 216  
217 217  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
218 218  
... ... @@ -242,10 +242,8 @@
242 242  ** drive the collimator in //IN// position
243 243  ** drive detector to 200 mm
244 244  
245 -
246 246  * Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
247 247  
248 -
249 249  //**Set run parameters and go 🏃💥**//
250 250  
251 251  1. Set your desired No. of frames
... ... @@ -347,7 +347,7 @@
347 347  {{layout-cell}}
348 348  ----
349 349  
350 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**14.7 Troubleshooting** ==
346 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**8.7 Troubleshooting** ==
351 351  
352 352  * (((
353 353  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ====
... ... @@ -356,7 +356,6 @@
356 356  * motor connected (icon green)?
357 357  )))
358 358  
359 -
360 360  * (((
361 361  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ====
362 362  
... ... @@ -365,7 +365,6 @@
365 365  * motor limits reached? → position displayed in red
366 366  )))
367 367  
368 -
369 369  * (((
370 370  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ====
371 371  
... ... @@ -374,7 +374,6 @@
374 374  * Nozzle or lines clogged? → flush with water, change nozzle
375 375  )))
376 376  
377 -
378 378  * (((
379 379  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ====
380 380  
XWiki.XWikiRights[0]
Allow/Deny
... ... @@ -1,0 +1,1 @@
1 +Allow
Levels
... ... @@ -1,0 +1,1 @@
1 +view,comment,edit
Users
... ... @@ -1,0 +1,1 @@
1 +XWiki.ahenkel