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Title
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1 -08. Serial Crystallography: CFEL TapeDrive
1 +10. Serial Crystallography: CFEL TapeDrive
Content
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9 9  
10 10  ----
11 11  
12 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**8.1 Sample characteristics and preparation** ==
12 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}**14.1 Sample characteristics and preparation** ==
13 13  
14 14  suspension of microcrystals, **at least** 200 µL with 20% crystal density (more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc.
15 15  
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22 22  
23 23  ----
24 24  
25 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**8.2 Connecting sample to ElveFlow, sample exchange** ==
25 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}**14.2 Connecting sample to ElveFlow, sample exchange** ==
26 26  
27 27  *
28 28  ** ==
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44 44  
45 45  ----
46 46  
47 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**8.3 TapeDrive operation** ==
47 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}**14.3 TapeDrive operation** ==
48 48  
49 49  *
50 50  ** ==
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116 116  be careful with -z, tape could be pushed out of focus
117 117  )))
118 118  
119 +
119 119  
120 120  )))
121 121  * [[image:attach:kamzik_nozzle.PNG||height="400"]]
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124 124  
125 125  * The chiller circulates fluid through the gas nozzle.
126 126  
128 +
127 127  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ====
128 128  
129 129  
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139 139  
140 140  ----
141 141  
142 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**8.4 Tape roll exchange** ==
144 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}**14.4 Tape roll exchange** ==
143 143  
144 144  The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s).
145 145  
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167 167  {{layout-cell}}
168 168  ----
169 169  
170 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**8.5 Chopper** ==
172 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}**14.5 Chopper** ==
171 171  
172 172  start chopper gui from terminal:
173 173  
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210 210  {{layout-cell}}
211 211  ----
212 212  
213 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**8.6 Data collection** ==
215 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}**14.6 Data collection** ==
214 214  
215 215  Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command:
216 216  
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240 240  ** drive the collimator in //IN// position
241 241  ** drive detector to 200 mm
242 242  
245 +
243 243  * Open beam shutter BS1 in //CrystalControl //or// P11 XRayFeed //
244 244  
248 +
245 245  //**Set run parameters and go 🏃💥**//
246 246  
247 247  1. Set your desired No. of frames
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343 343  {{layout-cell}}
344 344  ----
345 345  
346 -== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**8.7 Troubleshooting** ==
350 +== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Troubleshooting"/}}**14.7 Troubleshooting** ==
347 347  
348 348  * (((
349 349  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ====
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352 352  * motor connected (icon green)?
353 353  )))
354 354  
359 +
355 355  * (((
356 356  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ====
357 357  
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360 360  * motor limits reached? → position displayed in red
361 361  )))
362 362  
368 +
363 363  * (((
364 364  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ====
365 365  
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368 368  * Nozzle or lines clogged? → flush with water, change nozzle
369 369  )))
370 370  
377 +
371 371  * (((
372 372  ==== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues ====
373 373  
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