Changes for page CFEL TapeDrive: Serial Crystallography
Last modified by chatzies on 2025-11-27 11:35
Summary
-
Page properties (3 modified, 0 added, 0 removed)
-
Attachments (0 modified, 0 added, 22 removed)
- 20211201_094101.jpg
- 20211201_094111.jpg
- 20211201_095033.jpg
- 20211201_095205.jpg
- 20211201_095232.jpg
- 20211201_095534.jpg
- 20211212_233140.jpg
- Kamzik_run(2).PNG
- Screenshot from 2022-04-04 19-36-29.png
- TapeDrive coords.PNG
- TapeDrive scheme.png
- TapeDrive_beschriftet-tile.jpg
- TapeDrive_beschriftet.PNG
- kamzik_nozzle.PNG
- kamzik_run-tile.jpg
- kamzik_run.PNG
- kamzik_safety.PNG
- kamzik_tape.PNG
- safety_kamzik.PNG
- screen.PNG
- server client.PNG
- tape reset.PNG
-
Objects (1 modified, 0 added, 1 removed)
Details
- Page properties
-
- Title
-
... ... @@ -1,1 +1,1 @@ 1 - 08. Serial Crystallography: CFEL TapeDrive1 +14. Serial Crystallography: CFEL TapeDrive - Author
-
... ... @@ -1,1 +1,1 @@ 1 -XWiki. tabermah1 +XWiki.ahenkel - Content
-
... ... @@ -1,31 +1,81 @@ 1 1 {{layout}} 2 2 {{layout-section ac:type="single"}} 3 3 {{layout-cell}} 4 -[[image:attach:TapeDrive_beschriftet-tile.jpg||height=" 400"]]4 +[[image:attach:TapeDrive_beschriftet-tile.jpg||height="250"]] 5 5 6 +\\ 6 6 7 - {{toc/}}8 +\\ 8 8 10 +\\ 9 9 10 -- ---12 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.1RevertfromCrystallographytoTapeDrive(P11staff/CFEL)"/}}**14.1 Revert from Crystallography to TapeDrive (P11 staff/CFEL)** === 11 11 12 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14.1Samplecharacteristicsandpreparation"/}}8.1. Sample characteristics and preparation = 14 +* remove vortex 15 +* beamstop to out-position? 16 +* remove goniometer. The airbearing should be stopped (p11/servermotor/eh.1.01) 17 +* move cryojet out of the way, ramp the cryo up and shut it down. Close the compressed air to the shield flow. The biggest cable kinks and needs to be disconnected. 18 +* stop refill of the robot dewar and empty the dewar, warm up. 19 +* Disable backlight (unplug Festo connection). (% style="color: rgb(255,0,0);" %)//Is this still needed?// 20 +* (% style="color: rgb(0,0,0);" %)mount the 10 um diode and connect (via connector on the granite). This is connected to the leftmost Keithly (power up, check that settings are gain E06, Filter on, Rise time 1 ms. Keithly is connected to the oscilloscope and the delay generator, delay generator is connected to oscilloscope and detector, see diagram in P11 wiki. (% style="color: rgb(0, 0, 0); color: rgb(255, 0, 0)" %)//Insert here the setting for oscilloscope//(% style="color: rgb(0,0,0);" %)//. //Make sure to connect the multi-trigger to the back of the detector instead of the standard trigger, when starting to use the chopper (pull the thin ring with ‘grip’ area to detach). Cables are labeled. Make sure before using the chopper that the channels are enabled. 21 +* (% style="color: rgb(0,0,0);" %)move goniotower to X ~~ 17 000 13 13 14 - *Suspension ofmicrocrystals,**at least**200µLwith20%crystaldensity(moreisalwaysbetter),size range:2-30µm,**tip:** bringsomemother liquor forwashing,filtering,dilutingetc.23 +(% style="color: rgb(0,0,0);" %)Mounting of the TapeDrive is done by the CFEL group. Electronics and control units are combined on a small shelf, that requires only one power and network plug-in. The shelf will be placed left-sided (looking upstream) to the detector tower. The ElveFlow and control laptop as well as several necessary consumables are placed on a cart, which is to be positioned on the right (looking upstream) against the robot platform. The CFEL chiller is placed on the right of the platform and connected to the TapeDrive GASnozzle. 15 15 25 +\\ 26 + 27 +* adjust focus of the tape by moving X in goniometer tower until you see it in the overview camera. Final adjustment should be done when there is flow. Latest value is about 4500 in X and also 5000 in Z (higher soft limit changed from 2976,63 to 6000). (% style="color: rgb(255,0,0);" %)//Better to use the back illumination in the GUI to focus the tape - old instruction, not sure if this is the case. Back illumination is the external light source in the detector tower (the crystallography backlight should be disable for tapedrive).// 28 +* (% style="color: rgb(0,0,0);" %)Check the Minimum Detector Distance; the detector should not collide with the tapedrive while driven to 154 mm but it has to be verified. Also check that all cables and capillaries are taped away when the users start, so that nothing protrudes further than the tapedrive itself. Soft limit can be edited in eh.3.11 Atk panel. 29 +* (% style="color: rgb(0,0,0);" %)Reconfirm the alignment of the beamstop, once everything, including the nozzle, is in place. Modify config.ini for beamstop in- and out-position to both mach in (27 000). This way the beamstop will not be driven out when the hutch is opened, to avoid that the users forget to drive it in when restarting after entering the hutch. 30 + 31 +\\ 32 + 33 +Prepare necessary controls for data collection: 34 + 35 +* ATK panels: 36 +** p11/simplon_filewriter/eh.01 37 +** p11/simplon_detector/eh.01 38 +*** count time = 0.0075 39 +*** trigger (**ints **if working without the chopper, # or triggers is 1, **exts** if with the chopper, # or triggers = number of images). Exts is also the standard trigger in normal crystallography. If GUI is used to take images (e.g. for beamstop alignment) the trigger mode will be forced by that and needs to be reverted manually for the users to continue. 40 +*** numer of images = 100 000 41 +*** number of images in container = 1000 42 +*** mode 16m/4M 43 +*** detector distance = 200 mm (usually) 44 +** p11/detectortower 45 +** p11/motor/eh.09 46 +* remote access to TapeDrive control laptop: 47 +** open terminal, execute command: xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 48 + password: //written on control laptop 49 +// 50 +* Cameras: 51 +** haspp11ethcam1 → detector tower camera to monitor nozzle 52 +** haspp11ethcam4 → goniometer camera to monitor tape from above 53 +* OnDa (on haspp11user04): 54 +//This starts both GUIs (Frame Viewer & Crystallography GUI) and onda-monitor, the server component. The tool has a bunch of parameters which you can list with ./onda-runner.py —help.//\\ 55 +** 16M mode → cd /home/p11user/CfelSoft/202103_onda 56 + ./onda-runner.py onda-config/onda-config-Eiger16M.toml 57 +** 4M mode → cd /home/p11user/CfelSoft/202103_onda 58 + ./onda-runner.py onda-config/onda-config-Eiger4M.toml\\ 59 + 60 +\\ 61 + 62 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.2Samplecharacteristicsandpreparation"/}}**14.2 Sample characteristics and preparation** === 63 + 64 +suspension of microcrystals, **at least** 200 µL with 20% crystal density(more is always better), size range: 2-30 µm, **tip:** bring some mother liquor for washing, filtering, diluting etc. 65 + 16 16 Preparation: 17 17 18 -* filter through 30 µm (green) or 50 µm (yellow)cell filter intoanEppendorf or Falcon (original!) tube68 +* filter through 30 µm cell filter (green) into Eppendorf or Falcon (original!) tube 19 19 20 20 [[image:attach:20211201_095534.jpg||height="250"]] 21 21 72 +\\ 22 22 23 ----- 74 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.3ConnectingsampletoElveFlow,sampleexchange"/}}**14.3 Connecting sample to ElveFlow, sample exchange 75 +** === 24 24 25 - = {{id name="14.SerialCrystallography:CFELTapeDrive-14.2ConnectingsampletoElveFlow,sampleexchange"/}}8.2.Connectingsample toElveFlow,sample exchange=77 +After filtration, screw the ElveFlow connector to your Eppendorf or Falcon tube. Make sure that the yellow-ish line goes to the bottom of your tube. You can adjust the length by unscrewing the blue fitting on top and pushing/pulling the yellow-ish line. **Don't forget to tigthen the blue fitting afterwards!** 26 26 27 -After filtration, screw the ElveFlow connector to your Eppendorf or Falcon tube. Make sure that the yellow-ish tube goes all the way to the bottom of your tube. You can adjust the length by unscrewing the blue fitting on top and pushing/pulling the yellow-ish line. **Don't forget to tigthen the blue fitting afterwards!** 28 - 29 29 Be aware to which channel and nozzle line your sample is connected. 30 30 31 31 Red → Channel 1, crystal line (nozzle capillary without marks/with red marks) ... ... @@ -38,47 +38,44 @@ 38 38 39 39 [[image:attach:20211201_095232.jpg||height="250"]][[image:attach:20211201_095205.jpg||height="250"]] 40 40 91 +\\ 41 41 42 ----- 93 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.4TapeDriveoperation"/}}**14.4 TapeDrive operation 94 +** === 43 43 44 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14.3TapeDriveoperation"/}}8.3. TapeDrive operation = 45 - 46 -The TapeDrive is controlled through kamzik. To open kamzik, start the server. A terminal will open and shortly after a small window. 47 - 96 +The TapeDrive is controlled through kamzik. To open kamzik, start the server. A terminal will open and shortly after a small window. 48 48 Now start the client. Same thing, a terminal will open, shortly after a small window. 49 49 50 50 Click 'Devices' in the **client session** to open the control window. 51 51 [[image:attach:screen.PNG||height="250"]][[image:attach:server client.PNG||height="250"]] 52 52 53 - == {{id name="14.SerialCrystallography:CFELTapeDrive-Tape"/}}Tape ==102 +**Tape** 54 54 55 -* Click the 'main tape' icon 104 +* Click on the 'main tape' icon 56 56 * Change the velocity by typing anything from **0.3-3.0 mm/s** 57 57 * Common velocity is 1.0-1.5 mm/s 58 58 * kamzik displays the used tape in m and %. At 98% the tape will automatically stop since the rolls need to be exchanged at this point. 59 - 108 +\\ 109 +* [[image:attach:kamzik_tape.PNG||height="400"]] 60 60 61 - [[image:attach:kamzik_tape.PNG||height="400"]]111 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}**Sample nozzle** ==== 62 62 63 - 64 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Samplenozzle"/}}Sample nozzle == 65 - 66 -* Click on the 'nozzle' icon. 113 +* Click an the 'nozzle' icon. 67 67 * ((( 68 68 The nozzle position can be adjusted in xyz by clicking on the arrows up and down. (Double arrow = 10 steps). Step size can be varied, 1mm steps are rather big and should be used carefully. 69 69 The absolute position is **not calibrated** and therefore changes after each restart of kamzik. 70 70 71 71 72 -(% style="color: #ff0000" %)**!!! **(% style="color:#000000" %)**During data collection make sure in which direction you are movingthe nozzle, do not move nozzle into beam**(% style="color:#ff0000" %)**!!!**(%%)119 +(% style="color: rgb(255,0,0);" %)**!!! **(% style="color: rgb(255, 0, 0); color: rgb(0, 0, 0)" %)**During data collection make sure in which direction you are moving, do not move nozzle into beam**(% style="color: rgb(255,0,0);" %)** !!!**(%%) 73 73 \\Adjust the nozzle position by eye until it nearly touches the tape and roughly meets the X-ray interaction point. Then, move to the control hutch to use the on-axis microscope for fine adjustment. Move the nozzle tip to the beam position (red X) and write down the absolut nozzle position. From there move the nozzle in +x to your desired distance.Different distances combined with the tape speed result in several delay times for time-resolved experiments. 74 74 75 75 (% class="wrapped" %) 76 76 |=((( 77 - 124 +\\ 78 78 )))|=((( 79 79 direction 80 80 )))|=((( 81 -recommended step size 128 +recommended step size 82 82 for visual adjustment 83 83 )))|=(% colspan="1" %)((( 84 84 recommended step size ... ... @@ -113,33 +113,37 @@ 113 113 be careful with -z, tape could be pushed out of focus 114 114 ))) 115 115 116 - 163 +** 164 +\\** 117 117 ))) 166 +* [[image:attach:kamzik_nozzle.PNG||height="400"]] 118 118 119 - [[image:attach:kamzik_nozzle.PNG||height="400"]]168 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}**Temperature control/Chiller** ==== 120 120 121 - 122 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Temperaturecontrol/Chiller"/}}Temperature control/Chiller == 123 - 124 124 * The chiller circulates fluid through the gas nozzle. 125 125 126 - == {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}Gas nozzle ==172 +\\ 127 127 174 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Gasnozzle"/}}**Gas nozzle** ==== 128 128 129 - == {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}IR camera ==176 +\\ 130 130 178 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-IRcamera"/}}**IR camera** ==== 131 131 180 +\\ 181 + 132 132 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 133 133 134 134 xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 135 - password: //written on control laptop (changes every 6 months)// 185 + password: //written on control laptop (changes every 6 months) 186 +// 136 136 188 +\\ 137 137 190 +\\ 138 138 139 -- ---192 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Taperollexchange"/}}**14.5 Tape roll exchange** === 140 140 141 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14.4Taperollexchange"/}}8.4. Tape roll exchange = 142 - 143 143 The tape stops automatically at 98% used length, if you need to change the rolls for orther reasons, stop the tape (velocity = 0.0 mm/s). 144 144 145 145 * Remove the (almost) empty feeder roll by pulling it upwards. ... ... @@ -147,7 +147,7 @@ 147 147 * Get a new tape roll (bottom left on the cart). **Polypropylen 15 µm** 148 148 * Cut the first cm of the new tape roll, directly behind the black sticky part. 149 149 * Place new roll on roll holder and use sticky tape to attach the end of the old tape to the beginning of the new roll. 150 -* Open magnetic tape stabilizer on the **left side**. (% style="color:#ff0000" %)//!!!BEAMSTOP!!!//201 +* Open magnetic tape stabilizer on the **left side**. //!!!BEAMSTOP!!!// 151 151 * Start the tape (3mm/s). Once the connetion side has arrived at the collector roll, stop the tape (0mm/s). 152 152 * Again, cut the tape directly behind the connection side. Replace the the old roll with the **empty **one. Old roll can be discarded. 153 153 * Attach new tape to the empty roll by using some sticky tape. ... ... @@ -154,29 +154,32 @@ 154 154 * Close tape stabilizer. 155 155 * Reset tape counter in kamzik by clicking "<Call>" in "Main-Tape". 156 156 157 -**[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]][[image:attach:tape reset.PNG||height="250"]]** 208 +**[[image:attach:20211201_094101.jpg||height="250"]][[image:attach:20211201_094111.jpg||height="250"]][[image:attach:tape reset.PNG||height="250"]] 209 +** 158 158 159 - 211 +\\ 212 + 213 +\\ 214 + 215 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-"/}}** 216 +** === 160 160 {{/layout-cell}} 161 161 {{/layout-section}} 162 162 163 163 {{layout-section ac:type="single"}} 164 164 {{layout-cell}} 165 -- ---222 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.7Chopper"/}}**14.7 Chopper** === 166 166 167 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14.5Chopper"/}}8.5. Chopper = 168 - 169 169 start chopper gui from terminal: 170 170 171 171 (% class="code" %) 172 172 ((( 173 - cd /gpfs/local/shared/ChopperControl 228 + cd /gpfs/local/shared/ChopperControl 174 174 ))) 175 175 176 176 (% class="code" %) 177 177 ((( 178 178 python chopperControl.py 179 -\\ 180 180 ))) 181 181 {{/layout-cell}} 182 182 {{/layout-section}} ... ... @@ -189,75 +189,86 @@ 189 189 {{layout-cell}} 190 190 **Chopper → no Chopper** 191 191 192 -* decrease frequency by max. 10 Hz steps 246 +* decrease frequency by max. 10 Hz steps\\ 193 193 ** click arrow down 10x, "Set", arrow down 10x, "Set", .... 194 194 * at frequency = 10 Hz, click "Stop" 195 -* set "Hole" to <none> (% style="color: #ff0000" %)//Takes some minutes//249 +* set "Hole" to <none> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 196 196 197 -(% style="color: #000000" %)**no Chopper → Chopper**251 +(% style="color: rgb(0,0,0);" %)**no Chopper → Chopper** 198 198 199 -* (% style="color: #000000" %)set "Hole" to <Inner hole (largest)> (% style="color:#ff0000" %)//Takes some minutes//200 -* (% style="color: #000000" %)increase frequency by max. 10 Hz steps201 -** (% style="color: #000000" %)click arrow up 10x, "Set", arrow up 10x, "Set", .....202 -* (% style="color: #000000" %)//usually 130Hz, results in exposure time of 3.7 ms(technical exposure will always be 7.7 ms, since max. frame rate is 130 Hz//253 +* (% style="color: rgb(0,0,0);" %)set "Hole" to <Inner hole (largest)> (% style="color: rgb(255,0,0);" %)//Takes some minutes// 254 +* (% style="color: rgb(0,0,0);" %)increase frequency by max. 10 Hz steps 255 +** (% style="color: rgb(0,0,0);" %)click arrow up 10x, "Set", arrow up 10x, "Set", ..... 256 +* (% style="color: rgb(0,0,0);" %)//usually 133 Hz, results in exposure time of 3.7 ms// 203 203 {{/layout-cell}} 204 204 {{/layout-section}} 205 205 206 206 {{layout-section ac:type="single"}} 207 207 {{layout-cell}} 208 -- ---262 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.8Datacollection"/}}**14.8 Data collection** === 209 209 210 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14.6Datacollection"/}}8.6. Data collection = 211 - 212 212 Once the hutch is interlocked, set remote control to the TapeDrive laptop by opening a terminal and executing the following command: 213 213 214 214 (% class="code" %) 215 215 ((( 216 - xfreerdp +clipboard /size:1920x1080 /u: cfelusr /v:cfeld-tapetop268 + xfreerdp +clipboard /size:1920x1080 /u:Cfelusr /v:cfeld-pcx22611 217 217 password: written on control laptop (changes every 6 months) 218 218 ))) 219 219 220 - //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 272 + //>>usually the terminal is open, just repeat previous command with arrow up, enter and type in the password// 221 221 222 - 274 +\\ 275 + 276 +Click "Start" icon in kamzik. 277 + 278 +[[image:attach:kamzik_run-tile.jpg||height="400"]] 279 + 280 +---- 223 223 {{/layout-cell}} 224 224 {{/layout-section}} 225 225 226 -{{layout-section ac:type="two_ left_sidebar"}}284 +{{layout-section ac:type="two_equal"}} 227 227 {{layout-cell}} 228 228 **Check list:** 229 229 230 -(% style="color: #ff0000" %)//always after entering the hutch!//288 +(% style="color: rgb(255,0,0);" %)//always after entering the hutch!// 231 231 232 -(% style="color:#000000" %)Click "Run" icon in kamzik. 290 +* Open BS1 (//CrystalControl)// 291 +* Put collimator in (//CrystalControl)// 292 +* Check beamstop position = 27 000 (//Atk panel p11/motor/eh.3.09)// 293 +* Open fast shutter (//CrystalControl)// 294 +* Check diode voltage ~~ 0.0 (//kamzik Run/Diode voltage)// 295 +* Close fast shutter (//CrystalControl)// 233 233 234 -* Put detector distance 200 in //prepare_for_measurement ( )// 235 -* Click "<Call>" next to //prepare_for_measurement// 236 -This will: 237 -** drive the collimator in //IN// position 238 -** drive detector to 200 mm 297 +\\ 239 239 240 -* OpenbeamshutterBS1 in //CrystalControl//or// P11XRayFeed //299 +**Set run parameters and go 🏃💥** 241 241 242 -//**Set run parameters and go 🏃💥**// 243 - 244 244 1. Set your desired No. of frames 245 -1. Enter the protein ID of your crystal sample 246 -1. Match exposure time with chopper setting or set desired exposure time 302 +1. Match exposure time with chopper setting 247 247 1. Check trigger setting and match to chopper setting 248 -no chopper → external triffer //off// 249 - chopper → external trigger// on// 250 -1. To start the run, click "<Call>" next to //start_run (exposure )// 251 -{{/layout-cell}} 304 +1. Set detector distance to 200.0 mm, confirm with //enter// and click "<Call>" button next to it. 305 +1. To start the run, click "<Call>" next to //exposure time// 252 252 253 -{{layout-cell}} 254 -[[image:attach:Kamzik_run(2).PNG]] 307 +\\ 308 + 309 +(% style="color: rgb(153,51,102);" %)**//Current bug~://** 310 + 311 +(% style="color: rgb(0,0,0);" %)You need to "Stop" run in kamzik manually after all images have been acquired. This moves the shield up and closes the fast shutter. Afterwards you can start a new run by clicking "<Call>". 312 + 313 + 314 +(% style="color: rgb(0,0,0);" %)Check progress in terminal with: 315 + 316 +(% class="code" %) 317 +((( 318 + cd /gpfs/current/raw/scan_frames 319 + watch "ls -lrt <run number>/ | tail" 320 +\\\\\\\\ 321 +))) 255 255 {{/layout-cell}} 256 -{{/layout-section}} 257 257 258 -{{layout-section ac:type="single"}} 259 259 {{layout-cell}} 260 -(% class="relative-table wrapped" style="width:55.9569%" %)325 +(% class="wrapped relative-table" style="width: 100.0%;" %) 261 261 |=((( 262 262 Parameter 263 263 )))|=((( ... ... @@ -268,7 +268,7 @@ 268 268 |((( 269 269 Images number 270 270 )))|((( 271 -number of frames you want to collect 336 +Set number of frames you want to collect 272 272 )))|(% colspan="1" %)((( 273 273 usually 100k - 200k, but adjust according to hitrate 274 274 ... ... @@ -279,9 +279,12 @@ 279 279 )))|((( 280 280 exposure time of Eiger 281 281 282 - 347 +\\ 283 283 )))|(% colspan="1" %)((( 284 -with chopper → opening time displayed in chopper GUI 349 +chopper at 133 Hz → 3.7 ms 350 + 351 +chopper at 66 Hz → 7.7 ms 352 + 285 285 no chopper → 7.7 ms 286 286 287 287 ---- ... ... @@ -291,7 +291,7 @@ 291 291 )))|((( 292 292 changes automatically 293 293 )))|(% colspan="1" %)((( 294 - 362 +\\ 295 295 ))) 296 296 |(% colspan="1" %)((( 297 297 Detector distance ... ... @@ -298,59 +298,44 @@ 298 298 )))|(% colspan="1" %)((( 299 299 current detector postion readout 300 300 )))|(% colspan="1" %)((( 301 - 369 +\\ 302 302 ))) 303 303 |(% colspan="1" %)((( 304 - proteinID372 +move_detector (distance) 305 305 )))|(% colspan="1" %)((( 306 - proteinID ofcrystal sample(see AMARCORD)374 +Set detector distance 307 307 )))|(% colspan="1" %)((( 308 - 376 +200.0 mm (% style="color: rgb(255,0,0);" %)confirm with //enter//, click "<Call>" 309 309 ))) 310 - 311 ----- 378 +|(% colspan="1" %)((( 379 +Diode voltage 380 +)))|(% colspan="1" %)((( 381 +read out of diode 382 +)))|(% colspan="1" %)((( 383 +**~~ 0 !!! higher values indicate missaligned beam stop!!! 384 +Call local contact 385 +** 386 +))) 312 312 {{/layout-cell}} 313 313 {{/layout-section}} 314 314 315 -{{layout-section ac:type="two_equal"}} 316 -{{layout-cell}} 317 -**After data collection/Before entering the exp. hutch:** 318 - 319 -1. Go to "Safety" in kamzik. 320 -1. Click "<Call>" next to //prepare_to_open_hutch. //This will automatically: 321 -11. Drive the collimator out 322 -11. Drive the detector back to 1500 mm 323 -1. Close beam shutter BS1 and break door interlock in //P11 XRayFeed //(monitor top left). 324 - 325 -[[image:attach:Screenshot from 2022-04-04 19-36-29.png]] 326 -{{/layout-cell}} 327 - 328 -{{layout-cell}} 329 - 330 - 331 - 332 - 333 - 334 - 335 -[[image:attach:safety_kamzik.PNG]] 336 -{{/layout-cell}} 337 -{{/layout-section}} 338 - 339 339 {{layout-section ac:type="single"}} 340 340 {{layout-cell}} 341 341 ---- 342 342 343 -= {{id name="14.SerialCrystallography:CFELTapeDrive-14. 7Troubleshooting"/}}8.7.Troubleshooting =394 +=== {{id name="14.SerialCrystallography:CFELTapeDrive-14.9Troubleshooting"/}}14.9 Troubleshooting === 344 344 345 345 * ((( 346 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped == 397 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Tapestopped"/}}Tape stopped ==== 347 347 348 348 * Tape roll empty? 349 349 * motor connected (icon green)? 350 350 ))) 351 351 403 +\\ 404 + 352 352 * ((( 353 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding == 406 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Nozzlemotorsarenotresponding"/}}Nozzle motors are not responding ==== 354 354 355 355 * displayed in green=connected? 356 356 * nozzle holder colliding somewhere? ... ... @@ -357,50 +357,15 @@ 357 357 * motor limits reached? → position displayed in red 358 358 ))) 359 359 413 +\\ 414 + 360 360 * ((( 361 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure == 416 +==== {{id name="14.SerialCrystallography:CFELTapeDrive-Sampleflowisnotrespondingtohigherpressure"/}}Sample flow is not responding to higher pressure ==== 362 362 363 363 * channel turned on? 364 364 * Sample empty? 365 365 * Nozzle or lines clogged? → flush with water, change nozzle 366 366 ))) 367 - 368 -* ((( 369 -== {{id name="14.SerialCrystallography:CFELTapeDrive-Simplonfilewriter/eigerstreamissues"/}}Simplon filewriter/eiger stream issues == 370 - 371 -* First, restart kamzik (server+client) and see if this solves the issue 372 -* If not, restart the Simplon server (in Astor → haspp11exp03, right click on Simplon/EH.1 and restart) 373 -* ((( 374 -If nothing works, kill the Simplon process and then start the server again:* 375 - 376 -((( 377 -(% class="code" %) 378 -((( 379 -ssh haspp11exp03 380 -))) 381 -))) 382 - 383 -* ((( 384 -(% class="code" %) 385 -((( 386 -ps -ef | grep Simplon 387 -))) 388 -))) 389 -* ((( 390 -(% class="code" %) 391 -((( 392 -kill -9 simplon_process_id 393 -))) 394 -))) 395 -))) 396 -* After the Simplon server is back up, close all kamzik windows and restart (first server, then client) 397 -))) 398 398 {{/layout-cell}} 399 399 {{/layout-section}} 400 - 401 -{{layout-section ac:type="single"}} 402 -{{layout-cell}} 403 - 404 -{{/layout-cell}} 405 -{{/layout-section}} 406 406 {{/layout}}
- 20211201_094101.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -5.8 MB - Content
- 20211201_094111.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -5.6 MB - Content
- 20211201_095033.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -3.1 MB - Content
- 20211201_095205.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -2.8 MB - Content
- 20211201_095232.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -7.2 MB - Content
- 20211201_095534.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -4.4 MB - Content
- 20211212_233140.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -6.5 MB - Content
- Kamzik_run(2).PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -134.4 KB - Content
- Screenshot from 2022-04-04 19-36-29.png
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -133.0 KB - Content
- TapeDrive coords.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -24.1 KB - Content
- TapeDrive scheme.png
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -114.3 KB - Content
- TapeDrive_beschriftet-tile.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -539.9 KB - Content
- TapeDrive_beschriftet.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -337.8 KB - Content
- kamzik_nozzle.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -120.5 KB - Content
- kamzik_run-tile.jpg
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -466.4 KB - Content
- kamzik_run.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -128.9 KB - Content
- kamzik_safety.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -139.1 KB - Content
- kamzik_tape.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -122.6 KB - Content
- safety_kamzik.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -126.9 KB - Content
- screen.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -94.0 KB - Content
- server client.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -262.2 KB - Content
- tape reset.PNG
-
- Author
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel - Size
-
... ... @@ -1,1 +1,0 @@ 1 -122.3 KB - Content
- Confluence.Code.ConfluencePageClass[0]
-
- Id
-
... ... @@ -1,1 +1,1 @@ 1 -23 50318051 +236824593 - URL
-
... ... @@ -1,1 +1,1 @@ 1 -https://confluence.desy.de/spaces/11/pages/23 5031805/14. Serial Crystallography: CFEL TapeDrive1 +https://confluence.desy.de/spaces/11/pages/236824593/14. Serial Crystallography: CFEL TapeDrive
- XWiki.XWikiRights[0]
-
- Allow/Deny
-
... ... @@ -1,1 +1,0 @@ 1 -Allow - Levels
-
... ... @@ -1,1 +1,0 @@ 1 -view,comment,edit - Users
-
... ... @@ -1,1 +1,0 @@ 1 -XWiki.ahenkel