Changes for page Sample environments

Last modified by fwilde on 2023/10/05 16:47
From version 7.1
edited by fwilde
on 2023/03/01 15:26
Change comment: There is no comment for this version
To version 10.1
edited by fwilde
on 2023/03/01 15:34
Change comment: There is no comment for this version

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1 -= {{id name="Sampleenvironments-Loadframe"/}}Load frame =
1 +A load frame, a furnace a hanging axis and a corrosions cell is available for users at the P05 micro tomography end station. Please contact the beamline staff is you want to use one of the sample envirnments.
2 2  
3 -A load frame is available for users at the P05 micro tomography end station. Please contact the beamline staff is you want to use the load frame
3 +== {{id name="Sampleenvironments-Loadframe"/}}Load frame ==
4 4  
5 5  * Forces up to 1 kN (both pushing or pulling)
6 6  * Load cells 20N, 50N, 100N, 200N, 500N and 100N available
... ... @@ -8,10 +8,32 @@
8 8  
9 9  [[image:attach:load_frame.png||height="250"]]
10 10  
11 -\\
11 +More information: Moosmann et al. "A load frame for in situ tomography at PETRA III", Proc. SPIE 11113, Developments in X-Ray Tomography XII, 1111318 (2019); [[https:~~/~~/doi.org/10.1117/12.2530445>>url:https://doi.org/10.1117/12.2530445||rel="nofollow" shape="rect"]]
12 12  
13 -= {{id name="Sampleenvironments-Mountingsampleenvironments"/}}Mounting sample environments =
13 +== {{id name="Sampleenvironments-Furnace"/}}Furnace ==
14 14  
15 +* Temperature up to 800°C
16 +* Two dependent heating zones
17 +* Sealed  gas chamber for gas infusion
18 +* Feed through rotation axis
19 +
20 +[[image:attach:furnace.jpg||height="400"]]
21 +
22 +== {{id name="Sampleenvironments-Hangingaxis"/}}Hanging axis ==
23 +
24 +* Sample immersion in fluids
25 +
26 +[[image:attach:hanging_axis_complete.jpg||height="250"]]
27 +
28 +== {{id name="Sampleenvironments-Corrosioncell"/}}Corrosion cell ==
29 +
30 +* Cell for corrosion experiments
31 +* "Headless" design for absorption contrast tomography
32 +
33 +[[image:attach:mgcorrcell.jpg||height="400"]]
34 +
35 += {{id name="Sampleenvironments-MountingUserprovidedenvironments"/}}Mounting User provided environments =
36 +
15 15  {{info}}
16 16  **If you plan to bring your own sample environment it is strongly recommended to contact the beamline staff weeks before the start of the beamtime.**
17 17  {{/info}}
... ... @@ -27,29 +27,29 @@
27 27  
28 28  [[image:attach:rotation_stage_drawing.png||height="250"]]
29 29  
30 -= {{id name="Sampleenvironments-Covers"/}}Covers =
52 +== {{id name="Sampleenvironments-Covers"/}}Covers ==
31 31  
32 32  For sample environments with liquids or any other materials that potentially spill, there are different 3 types of covers for the rotation stage. Each is explained in a section below which provides a technical drawing with drill patterns.
33 33  
34 -== {{id name="Sampleenvironments-Coverforassemblyonthesamplestage(piezostackalignment)"/}}Cover for assembly on the sample stage (piezo stack alignment) ==
56 +=== {{id name="Sampleenvironments-Coverforassemblyonthesamplestage(piezostackalignment)"/}}Cover for assembly on the sample stage (piezo stack alignment) ===
35 35  
36 36  This cover is intended for very small and light sample environments (less than 100g). The cover consists of three pieces. The top pieze sits on the [[sample stage>>doc:P5I.Instrumentation.P05 experimental hutch 2.Sample stage.WebHome]] and allows for adjustment of the sample environment w.r.t. the rotation axis.
37 37  
38 38  {{view-file att--filename="Spritzschutz-dreiteilig.pdf" display="thumbnail" height="250"/}}{{view-file att--filename="Spritzschutz-dreiteilig-Bohrbild.pdf" display="thumbnail" height="250"/}}
39 39  
40 -== {{id name="Sampleenvironments-Coverforsamplemountoninner(precise)rotationstage"/}}Cover for sample mount on inner (precise) rotation stage ==
62 +=== {{id name="Sampleenvironments-Coverforsamplemountoninner(precise)rotationstage"/}}Cover for sample mount on inner (precise) rotation stage ===
41 41  
42 42  This cover carries bulkier sample enviroments (less than 2 kg). It consists of two pieces, the inner piece sitting on the air bearing precise inner rotation stage. High precision rotation is thus maintained, but alignment w.r.t. to the rotation axis is not possible (but can be realized by the sample environment itself).
43 43  
44 44  {{view-file att--filename="Spritzschutz-zweiteilig.pdf" display="thumbnail" height="250"/}}{{view-file att--filename="Spritzschutz-zweiteilig-Bohrbild.pdf" display="thumbnail" height="250"/}}
45 45  
46 -== {{id name="Sampleenvironments-Coverforsamplemountonouter(heavyduty)rotationstage"/}}Cover for sample mount on outer (heavy duty) rotation stage ==
68 +=== {{id name="Sampleenvironments-Coverforsamplemountonouter(heavyduty)rotationstage"/}}Cover for sample mount on outer (heavy duty) rotation stage ===
47 47  
48 48  This cover consists of only on piece sitting on the outer, roller bearing rotation stage. High rotation precision is not maintained, but the cover carries heavier loads.
49 49  
50 50  {{view-file att--filename="Spritzschutz-einteilig.pdf" display="thumbnail" height="250"/}}{{view-file att--filename="Spritzschutz-einteilig-Bohrbild.pdf" display="thumbnail" height="250"/}}
51 51  
52 -== {{id name="Sampleenvironments-Overviewofrotationstagecovers"/}}Overview of rotation stage covers ==
74 +=== {{id name="Sampleenvironments-Overviewofrotationstagecovers"/}}Overview of rotation stage covers ===
53 53  
54 54  {{view-file att--filename="Spritzschutz-Vergleich.pdf" display="thumbnail" height="250"/}}
55 55  
Confluence.Code.ConfluencePageClass[0]
Id
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1 -297521477
1 +326975404
URL
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1 -https://confluence.desy.de/spaces/P5I/pages/297521477/Sample environments
1 +https://confluence.desy.de/spaces/P5I/pages/326975404/Sample environments